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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3 <br />Job Number: C17728 <br />Account: GEAICAO Giles Engineering Associates, Inc. <br />Project: 239 West 11th Street - Tracy, CA <br />Sample <br />File ID <br />DF <br />Analyzed <br />By <br />Prep Date <br />Prep Batch <br />Analytical Batch <br />C17649-12MS <br />L10266.D <br />1 <br />09/02/11 <br />TF <br />n/a <br />n/a <br />VL321 <br />C17649-12MSD <br />L10267.D <br />1 <br />09/02/11 <br />TF <br />n/a <br />n/a <br />VL321 <br />C17649-12 <br />L10262.D <br />1 <br />09/02/11 <br />TF <br />n/a <br />n/a <br />VL321 <br />The QC reported here applies to the following samples: Method: SW846 8260B <br />C17728-1, C17728-2, C17728-3, C17728-4 <br />ED 27 of 29 <br />w ACCLJTEBT. <br />c17728 1..1-- - <br />C17649-12 <br />Spike <br />MS <br />MS <br />MSD <br />MSD <br />Limits <br />CAS No. <br />Compound <br />ug/1 Q <br />ug/1 <br />ug/1 <br />% <br />ug/1 <br />% <br />RPD <br />Rec/RPD <br />67-64-1 <br />Acetone <br />ND <br />80 <br />55.3 <br />69 <br />59.3 <br />74 <br />7 <br />60-130/25 <br />71-43-2 <br />Benzene <br />ND <br />20 <br />18.2 <br />91 <br />18.0 <br />90 <br />1 <br />60-130/25 <br />108-86-1 <br />Bromobenzene <br />ND <br />20 <br />20.4 <br />102 <br />20.5 <br />103 <br />0 <br />60-130/25 <br />74-97-5 <br />Bromochloromethane <br />ND <br />20 <br />20.0 <br />100 <br />20.1 <br />101 <br />0 <br />60-130/25 <br />75-27-4 <br />Bromodichloromethane <br />ND <br />20 <br />20.1 <br />101 <br />19.7 <br />99 <br />2 <br />60-130/25 <br />75-25-2 <br />Bromoform <br />ND <br />20 <br />22.3 <br />112 <br />21.8 <br />109 <br />2 <br />60-130/25 <br />104-51-8 <br />n-Butylbenzene <br />ND <br />20 <br />16.6 <br />83 <br />16.8 <br />84 <br />1 <br />60-130/25 <br />135-98-8 <br />sec-Butylbenzene <br />ND <br />20 <br />17.8 <br />89 <br />18.0 <br />90 <br />1 <br />60-130/25 <br />98-06-6 <br />tert-Butylbenzene <br />ND <br />20 <br />17.9 <br />90 <br />18.2 <br />91 <br />2 <br />60-130/25 <br />108-90-7 <br />Chlorobenzene <br />ND <br />20 <br />19.5 <br />98 <br />19.5 <br />98 <br />0 <br />60-130/25 <br />75-00-3 <br />Chloroethane <br />ND <br />20 <br />18.8 <br />94 <br />18.4 <br />92 <br />2 <br />60-130/25 <br />67-66-3 <br />Chloroform <br />ND <br />20 <br />18.4 <br />92 <br />18.3 <br />92 <br />1 <br />60-130/25 <br />95-49-8 <br />o-Chlorotoluene <br />ND <br />20 <br />18.2 <br />91 <br />19.7 <br />99 <br />8 <br />60-130/25 <br />106-43-4 <br />p-Chlorotoluene <br />ND <br />20 <br />17.3 <br />87 <br />17.7 <br />89 <br />2 <br />60-130/25 <br />56-23-5 <br />Carbon tetrachloride <br />ND <br />20 <br />18.5 <br />93 <br />18.2 <br />91 <br />2 <br />60-130/25 <br />75-34-3 <br />1,1-Dichloroethane <br />ND <br />20 <br />17.9 <br />90 <br />17.7 <br />89 <br />1 <br />60-130/25 <br />75-35-4 <br />1,1-Dichloroethylene <br />ND <br />20 <br />15.4 <br />77 <br />15.4 <br />77 <br />0 <br />60-130/25 <br />563-58-6 <br />1,1-Dichloropropene <br />ND <br />20 <br />17.9 <br />90 <br />17.6 <br />88 <br />2 <br />60-130/25 <br />96-12-8 <br />1,2-Dibromo-3-chloropropane <br />ND <br />20 <br />17.5 <br />88 <br />17.4 <br />87 <br />1 <br />60-130/25 <br />106-93-4 <br />1,2-Dibromoethane <br />ND <br />20 <br />21.1 <br />106 <br />20.7 <br />104 <br />2 <br />60-130/25 <br />107-06-2 <br />1,2-Dichloroethane <br />ND <br />20 <br />20.3 <br />102 <br />19.7 <br />99 <br />3 <br />60-130/25 <br />78-87-5 <br />1,2-Dichloropropane <br />ND <br />20 <br />20.0 <br />100 <br />19.7 <br />99 <br />2 <br />60-130/25 <br />142-28-9 <br />1,3-Dichloropropane <br />ND <br />20 <br />20.8 <br />104 <br />20.8 <br />104 <br />0 <br />60-130/25 <br />108-20-3 <br />Di -Isopropyl ether <br />ND <br />20 <br />18.1 <br />91 <br />18.1 <br />91 <br />0 <br />60-130/25 <br />594-20-7 <br />2,2-Dichloropropane <br />ND <br />20 <br />15.1 <br />76 <br />14.8 <br />74 <br />2 <br />60-130/25 <br />124-48-1 <br />Dibromochloromethane <br />ND <br />20 <br />20.3 <br />102 <br />20.4 <br />102 <br />0 <br />60-130/25 <br />75-71-8 <br />Dichlorodifluoromethane <br />ND <br />20 <br />20.0 <br />100 <br />19.3 <br />97 <br />4 <br />60-130/25 <br />156-59-2 <br />cis-1,2-Dichloroethylene <br />ND <br />20 <br />18.3 <br />92 <br />18.2 <br />91 <br />1 <br />60-130/25 <br />10061-01-5 <br />cis-1,3-Dichloropropene <br />ND <br />20 <br />20.8 <br />104 <br />20.4 <br />102 <br />2 <br />60-130/25 <br />541-73-1 <br />m -Dichlorobenzene <br />ND <br />20 <br />19.1 <br />96 <br />19.2 <br />96 <br />1 <br />60-130/25 <br />95-50-1 <br />o -Dichlorobenzene <br />ND <br />20 <br />19.5 <br />98 <br />19.8 <br />99 <br />2 <br />60-130/25 <br />106-46-7 <br />p -Dichlorobenzene <br />ND <br />20 <br />19.1 <br />96 <br />19.4 <br />97 <br />2 <br />60-130/25 <br />156-60-5 <br />Vans-1,2-Dichloroethylene <br />ND <br />20 <br />16.9 <br />85 <br />16.6 <br />83 <br />2 <br />60-130/25 <br />10061-02-6 <br />trans-1,3-Dichloropropene <br />ND <br />20 <br />20.5 <br />103 <br />20.3 <br />102 <br />1 <br />60-130/25 <br />100-41-4 <br />Ethylbenzene <br />ND <br />20 <br />18.7 <br />94 <br />18.6 <br />93 <br />1 <br />60-130/25 <br />637-92-3 <br />Ethyl Tort Butyl Ether <br />ND <br />20 <br />19.6 <br />98 <br />19.7 <br />99 <br />1 <br />60-130/25 <br />ED 27 of 29 <br />w ACCLJTEBT. <br />c17728 1..1-- - <br />