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TABLE 4 Page 6 of 9 SOIL DATA INDEPENDENT SHELL-BRANDED SERVICE STATION 4315 WATERLOO ROAD STOCKTON,CALIFORNIA Sample Ethyl- MTBE MTBE Sample Depth Date TPHg Benzene Toluene benzene Xylenes 8020 8260 DIPE ETBE TAME TBA 1,2-DCA EDB Ethanol Lead Comments ID (fbg) Sampled mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg S-7-12.0 12 2-Apr-05 <1.0 <0.0050 <0.0050 <0.0050 <0.0050 --- <0.0050 - - - - - - Over-excavation sample 58.12,0 12 2-Apr-05 11,000 0.88 67 180 1,000 - <0.25 - - - -- - - - - Over-excavation sample S-9-12.0 12 2-Apr-05 5,200 <0.10 0.24 12 160 - <0.10 - - - - - - - - Over-excavation sample f'l 510-12.0 12 2-Apr-05 1,900 0.020 <0.0050 0.82 5.7 - <0.0050 - - - - - - - - Over-excavation sample 511-12.0 12 2-Apr-05 3,600 0.65 14 31 330 - <0.15 - - - -- - - - - Over-excavation sample __ ver-excavation sam e - - - - - - - - _l'... 512-7.0 � 7 pr- _ 170 <0.025 <11.025 1.4 2.2 - <0.025 ver-excavation sam e 513-7.0 �7f-�r� 1�4 _<O.U050 <O.OU50 0.031 <0.0050 --- _0.015 _��_-_ - �_ --_.._..,.._. -� -` � --' .� 514.9.0 7 5-Apr-05 <1.0 <0.0050 <0.0050 <0.0050 <0.0050 --- 0.013 -- - - - - - - Over-excavation sample -- __ ___ er-ex --- vcavation sam _ e 5 .00 15-4.0 �4�- Tr7�r '-T 16133 <051) 14-__ 0.017_-- - --0.042- -- - ----------- -...�. _ �. . � . �a 516-7.00.036 <0.025._14 66 1.1 __ ---_ - erexcavaiionsam c 517-11.5 11.5 5-Apr-05 680 0.044 0.45 9.3 55 - <0.025 - - - - - - - - Over-excavation sample 518-11.5 11.5 5-Apr-05 <1.0 <0.0050 <0.0050 0.0056 0.025 - <0.0050 - - - - - - - - Over-excavation sample SB-11-7 7 12-Dec-05 <1.0 <0.0050 <0.0050 <0.0050 <0.0050 - 0.066 <0.010 <0.0050 <0.0050 0.049 <0.0050 <0.0050 - - SB-11-10 10 12-Dec-05 <1.0 <0.0050 <0.0050 <0.0050 <0.0050 - 0.11 <0.010 <0.0050 <0.0050 <0.010 <0.0050 <0.0050 -- - SB-11-12 12 12-Dec-05 <1.0 <0.0050 <0.0050 <0.0050 <0.0050 -- 0.088 <0.010 <0.0050 <0.0050 0.16 <0.0050 <0.0050 - - SB-11-20 20 12-Dec-05 <5.0 <0.025 <0.025 <0.025 <0.025 - 1.4 <0.050 <0.025 <0.025 0.31 <0.025 <0.025 - - SB-11-30 30 12-Dec-05 <50 <0.50 <0.50 <0.50 <0.50 - 2.7 <1.0 <0.50 <0.50 <2.5 <0.50 <0.50 - SB-11-40 40 12-Dec-05 <1.0 <0.0050 <0.0050 <0.0050 <0.0050 - 0.31 <0.010 <0.0050 <0.0050 0.23 <0.0050 <0.0050 - SB-11-50 50 12-Dec-05 <2.5 <0.013 <0.013 <0.013 <0.013 - 0.32 <0.025 <0.013 <0.013 0.26 <0.013 <0.013 --- SB-11-60 60 12-Dec-05 <4.7 <0.024 <0.024 <0.024 <0.024 - 0.77 <0.047 <0.024 <0.024 0.53 <0.024 <0.024 - -- SB-12-5 5 12-Dec-05 <1.0 <0.0050 <0.0050 <0.0050 <0.0050 --- 0.013 <0.010 <0.0050 <0.0050 <0.010 <0.0050 <0.0050 --- SB-12-7 7 12-Dec-05 <1.0 <0.0050 <0.0050 <0.0050 <0.0050 --- 0.0086 <0.010 <0.0050 <0.0050 <0.010 <0.0050 <0.0050 - - SB-12-10 10 12-Dec-05 1.1 <0.0050 <0.0050 <0.0050 <0.0050 - 0.0056 <0.010 <0.0050 <0.0050 0.019 <0.0050 <0.0050 - SB-12-15 15 12-Dec-05 1,800 <2.5 <2.5 7.2 81 - 9.0 <5.0 <2.5 <2.5 <13 <2.5 <2.5 - SB-12-25 25 12-Dec-05 <4.6 <0.023 <0.023 <0.023 <0.023 -- 1.1 <0.046 <0.023 <0.023 0.051 <0.023 <0.023 - - SB-12-35 35 12-Dec-05 <50 <0.50 <0.50 <0.50 <0.50 - 15 <1.0 <0.50 <0.50 <2.5 <0.50 <0.50 - - SB-12-45 45 12-Dec-05 <50 <0.50 <0.50 <0.50 <0.50 - 1.2 <1.0 <0.50 <0.50 <2.5 <0.50 <0.50 - - 247359(17)