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885]aryls Chive <br /> Sequoia Morgan Hili CA 95037 <br /> (408)77&%00 <br /> Analytical <br /> FAX(408)782-6308. seciuolalabs corn <br /> • <br /> Blaine Tech Services(Shell) Project 43I5 Waterloo <br /> 1680 Rogers Avenue Project Number 4315 Waterloo/Stockton Reported <br /> San Jose CA,95112 Project Manager Nick Sudano 11/09/00 15 54 <br /> MTBE by EPA Method 8260B- Quality Control <br /> Sequoia Analytical- San Carlos <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Lima Notes <br /> Batch 0110016-EPA 5030B [P/Ti <br /> Blank(0110016-BLK1) Prepared&Analyzed 11/02/00 <br /> Methyl tert-butyl ether ND 200 ug/I <br /> Surrogate 1 2-Dichloroethane-d4 520 500 104 760-114 <br /> LCS(0110016-BSI) Prepared&Analyzed 11/02/00 <br /> Methyl tert-butyl ether 483 200 ug/I 500 966 700-130 <br /> Surrogate 11-Dichloroethane-d4 540 500 108 760-114 <br /> Matrix Spike(0110016-MSI) Source:L011006-03 Prepared&Analyzed 11/02/00 <br /> Methyl tert-butyl ether 519 200 ug/1 500 ND 104 600-140 <br /> Surrogate 12-Dichloroethane-d4 525 500 105 760-114 <br /> x Spike Dup(0110016-MSD1) Source:LOI1006-03 Prepared&Analyzed 11/02/00 <br /> yl tert-butyl ether 519 200 ug/I 500 ND 104 600-140 0 250 <br /> Surrogate 12 Dichloroethane-d4 518 500 104 76 0-I14 <br /> oia Analytical-Morgan Hill The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document 77us analytical report must be reproduced in its entirety <br /> Page 5 of 6 <br />