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i <br /> X-N <br /> i 455 McDowell Blvd North Ste D <br /> Sequoia Petaluma CA 94954 <br /> (707) 792-1865 <br /> Analytical FAX(707) 792-0342 <br /> IV <br /> Cambria Environmental Project Shell Oil Co Sampled 9115199 <br /> 270 Perkins St Project Number 4315 Waterloo Received 9/16/99 <br /> Sonoma,CA 95476 Project Manager Bob Perlowski Reported 9/29/99 <br /> Volatile Organic Compounds by EPA Method 826013 <br /> Sequoia Analytical-Petaluma <br /> Batch Date Date Surrogate Reporting <br /> Analyte Number Prepared Analyzed Limits Limit Result Units Nates* <br /> MW1-40 P909531-07 Soil <br /> Tert-amyl methyl ether 9090574 9123/99 9/23/99 000500 ND mg/kg <br /> Tert-butyl alcohol 0 t00 ND <br /> Di-isopropyl ether 000500 ND " <br /> 1,2-Dibromoethane(EDB) 000500 ND " <br /> 1,2-Dichloroethane 000500 ND " <br /> Ethyl tert-butyl ether 000500 ND " <br /> Methyl tert-butyl ether 000500 00208 " <br /> Surrogate Dibromofluoromethane 800-120 98 0 <br /> Surrogate 12-Dichloroethane-d4 lo " 800-120 970 " <br /> Surrogate Toluene-d8 11 11810-117 102 <br /> Surrogate 4-Bromofluorobenzene 740-121 996 " <br /> MWI-65 P909531-12 Soil <br /> T"yl methyl ether 9090574 9/23/99 9/23/99 000500 ND mg/kg <br /> I'MMtyl alcohol 0 100 ND <br /> Di-isopropyl ether 000500 ND " <br /> 1,2-Dibromoethane(EDB) 000500 ND " <br /> 1,2-Dichloroethane 000500 ND " <br /> Ethyl tert-butyl ether 000500 ND " <br /> Methyl tert-butyl ether _ _ __ _ 000500 ND_ <br /> Surrogate Dibromofluoromethane 800-120 932 <br /> Surrogate 12-Dichloroethane-d4 800-120 92 8 <br /> Surrogate Toluene-d8 " " 1181 0-117 98 6 " <br /> Surrogate 4-Bromofluorobenzene 740-121 962 <br /> MW 1-75 P909531-14 Soil <br /> Tert-amyl methyl ether 9090574 9123199 9/23199 000500 ND mg/kg <br /> Tert-butyl alcohol 0 too ND " <br /> Di-isopropyl ether 000500 ND " <br /> 1,2-Dibromoethane(EDB) 000500 ND " <br /> 1,2-Dichloroethane 000500 ND " <br /> Ethyl tert-butyl ether 000500 ND " <br /> Methyl cert-butyl ether 000500 ND _ <br /> Surrogate Dibromofluoromethane 800-120 94 0 <br /> Surrogate 12-Dichloroethane-d4 800-120 962 " <br /> Surrogate Toluene-d8 810-117 978 <br /> Surrogate 4-Bromofluorobenzene 740-121 95 6 " <br /> Sequoia Analytical- Petaluma *Refer to end of report for tent of notes and dcfanition-s <br /> Page 3 of 7 <br />