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mar VERIFICATION LABORATORY WYSIS TANK TANK TPH-G TPH-D BTX & E CL HC TOTAL MTBE METALS PCB N CONTENTS 8015 8015 8020 8010 LEAD Ta^•e" ICAP/ 8270 8260 8260 8260 8240 7420 re AES or 8080 7421 8020 AA 8260 LEADED GAS X X X X UNL GAS X X X DIESEL X X KEROSENE X X UNK FUEL X X X X X PROD. OIL X X CHLOR. i SOLVENTS ,X X NONCHLOR SOLVENTS X X X W ASl'E1 nsrn ott. r X X X r All analysis methods are the designated EPA methods described in EPA SW 846, Third Edition. Those methods not found In SW 846 are specifically noted below. Refer to the "SWRCB LUFT Field Manual", Appendix D (B), Table 3-5 on page A20 for mininnnn detection limits for motor vehicle fuel (gasoline and diesel). Refer to 1-2-3 'Regional Board Staff Recommendations for Initial Evaluation and Investigation of UST's" for the waste and motor oil minimum detection limits. Detection Limits thnt remnin below the MCL, STLC or Allowable Limit of the contaminant in question will be accepted, however laboratory shall utilize the most conservative method. I LATIORA FURY ANALYSES TERMINOLOGY: TPit-G Total Petroleum Hydrocarbon, Gasoline, GC/FID (5030) 8015 mod or GUMS 8260 1 PTI IT Total Petroleum Hydrocarbon, Diesel, GC/FID (3550), 8015 mod or GUMS 8260 BTX & E Benzene, Toluene, Xylene & Ethyl Benzene, GC/PID 8020 or GC/MS 8260 CL TIC Chlorinated Hydrocarbon, GC/HSD 8010, GC/MS 8240 TOTAL L.FAD Total lead, AA 7420, AA 7421 or ICP-AES 6010 M1 BE Methyl Tertiary Butyl Ether, GC/PID 8020 and confirmed by GUMS 8260 MF_TALS [CAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Spectrometry 7000. Metals: Cadmium, Chromium III and VI, Lead, Zine and Nickel. PCB Polychlorinated Biphenyls, GC/MS 8270 or 8080 GC FID Gas Chromatography, Flame Ionization Detection Method 3050 Acid digestion Method 3540 Soxhlet sample preparation Method 3550 Sonication sample preparation, extraction method Method 5030 Purge and trip sample preparation QA/QC Quality Assurance/Quality Control Nntc : L0 avoid false positive detection of benzene, benzene-Gee solvents are to be used. Fused capillary columns are preferred to packed columns; a packed column may be used as a "first cut' with 'dirty' samples or once the hytyoearbone have been characterized and proper QA/QC is followed. ror drinking water sources, FPA recommends that the 500 series for volatile organic should be used in preference to the 600 series because the, detection limits are lower and the QA/QC is better. Samples exhibiting any level of heavy metal contamination may require further analysis. PHS-EHD recommends holding those samples until disposal is indicated. Ell 23 046 (Revised (0%24/97) Page 9