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10/17/2008 89;00 2094683433 FIFTH FLOOR <br /> PACS 08 <br /> r1 1M VERxFJCATIC?i LABORATORY ANALYSIS <br /> TANK TPH-G TPH-D BTX do E CL HC TOTAL MTBE (MTBE-.ran inx <br /> ,lt CONTENTS Sols 8015 8020 8010 LEADam FTSE,TJWDIP'E. IC"/ I'C$ <br /> 8260 8260 8250 8240 742Q 8260 AES 8270 <br /> 8260 7421 am 1 or 8080 <br /> 6. A,s► <br /> LEADED©AS X X X X <br /> UNL GAS x x X <br /> DIESEL x X <br /> KEROSENE x x x <br /> UNK FUEL. x x x x x <br /> PROD 01L x x x <br /> CHLOR. x <br /> SOLVENTS x x <br /> NONCHLOR X <br /> SOLVENTS x x <br /> WASTE\ <br /> USED OJL x x x X Tx x x <br /> A11 analysis methods are dw deskpAted EPA methods d-serilicd in EPA SW Bab. Third Editioat. These rA ;!-s tint found in SW <br /> 846 a*speclfcsuy netedbelow. Refer to Me --SWRCB LUFT Field Manual", ApD(B),Table 3-5 on pne A20 for <br /> mimnmutn demctioa limits for mawr vehicleAwl (psollne and dkse=i). Refer to"Tri Ite&nai Board ftff Recmtumandnions for <br /> Aftal Evalttatim and Investiption of UST'x- lips tree waste orad motor ad MW==3e=tkm limas <br /> IWINIM Umks Mat regain bebw the MCL. STLC or Atlawabh mit or the cornta-1—ist in question w111 be accepted, <br /> > owe+rer labundory zbAU udlin the nmm commrvaiive=colwd <br /> LA2KMA'TORY ANALYSES TVU41NOU)GY. <br /> TPH-G Total pcuoloura 3iydrocarbm Crasclbw,OCIFM(500)SOIS scrod or GGMS 8260 <br /> TPH D Tout Pcrroleum Eydrocarboa Diesel,CCrFID(3350), 8413 mod or GC/MS SM <br /> BTT{&E Bem=is. Totueftc, Xylcne dt F.tk*ll Benzene. 0ClPIn 8020 or OClMS 8X30 <br /> CL HC Chlorinated Hydrocarbon. GC/HSD 8010. G0MS 8740 ar 8M0 <br /> TOTAL LEAD Total lead. AA 742+0. AA 7421 or ICP-ASS 6010 <br /> OXYGENATES MTBE,ETBE.TAME.D11PE,8c TIM G41MS 9260(For MTSE screen only you may use 8020) <br /> METALS ICAP pr AA Inductively Coupled plasma Atornic FsmiWoa Spectrom try 6010 or Atomic Absorpum Sp=xom=y 7000. <br /> blstab-C.adrvits . Chromium m and VI,Lead,zinc and NIdW <br /> FCB T'blychlorh atcd Biphem►ls. GCrMS aM or soda <br /> GC-PID Gas ChriorrnwpwphDe, Flaunt kni=don Deacum <br /> Method 3050 Aeld deestion <br /> bftxhod 3540 Bomb et sample preparation <br /> bfcdwd 3550 Someation umple preparatim extraction method <br /> Method 5030 Purge and UV ;WmWaten <br /> QAJQ'C Quality Asstuancelou"tty Comroi <br /> ;:CIU*- 1 e avo.o raise positive aetecaon of benzene.betUern-free solvents are w be used ftsea capillary columns are preferred to pacw <br /> column!;a packed oohum may be used as a'first cur'with dirty'samples or mtoa the hydrocarbons haw!teen c?iaraaeelzad and FmPcr <br /> QAIQC is foUawed. <br /> For drinking water sources, EPA recornmends that the SM series for volatile oraanlo should be used In prcferenw to the 640 seises ber3use the <br /> detection limas arc lower and chc QA/QC is better. Samples exh3ibipng any level of heavy rwr l cornarsaration may require ltwther analysis <br /> PH-"-MM reeommceds holding triose sampics until disposal b mdieatad <br /> EK 23 046 (Revised 05M9100) Page a <br />