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yrs }� p� q <br /> '� c�i.t`�. b e.I t'�ar<alyfica�l' Ing., 1534 Wil-'Olt PassAoad P:t1rhilrg,CA 94565-'1701 <br /> - 4Veh:nwxc.mccmnpi:°ll cOm !-u:ail:n7ar{n�veearnnbelLcum <br /> ( _ "Ii7:antnraEitx�'.o!uitt` 'I'dc lion. X77 !) �' spas '.r -q - <br /> W.O.Sample Matrix: Sail QC Matrix Soil WorkOrder 0705161 <br /> . ....,.:�....-----_-..._.M.�.. _ _ <br /> EPA Method SM53106 Extraction SM5310D OatcltlD; 27894 <br /> Spiked.Sample ID: 0705169-003A <br /> Analyte Sample Spiked MS A/8C MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(°�) <br /> n7glKg mg/Kg Rec, q/o f�ec. °ti RPD °6 Rec. °G Rac. %Rpb MS MSD RPDLC$YLCSD RPD <br /> TOC 2600 82l)[S 93.8 95 0.969 103 ]U3 ll 7q- 13D 20 80 -720 20 <br /> All target cnmptinndH in the MethodBlank of this extraction batch were ND less than the m <br /> NONE ethod Ri,with Chu Following exr eplions: <br /> f <br /> SA7ClLZ7894 SLIAlI ARY <br /> Sample ID Dafe Sampled Date Extracted Date Analyzed Sam #e ID <br /> p Data Sampled bate-Extracted Date Analyzed <br /> 0705161-QU.A U5/D4/07 9:47 AM 05/03/07 05108/0-17,i.4 PVf 0705161-005A 65/01107 12:12 PM 05/08/07 05/08/07 8:58 PM <br /> r- <br /> r <br /> 1 <br /> [=am <br /> x.Spike;MSD-Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=l.aboralnry Control Sample Duplicate;RPD=Relative <br /> cent peviatlon, <br /> ry=100"{MS-Sample)/(Amount Spiked] PPD=10D"(MS- MSD)/((MS+MSt7)/2). <br /> spike recoveries and/or;%RPD nay Carl"si=ze of[aboretery acceptance niter&due tc one or more of the following reasnns:a)the sample is Inhomogerhrms AND i <br /> gn cant concentrations of analytn relative to the amount spiked;or b)the spiked sample's matTN Mierferes wilts the spike recovery.' <br /> NIApplicable to this method, <br /> te concentration}n sample exceeds spi e amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to thigh matrix or analyte content. <br /> u� <br /> DHS FLAP Certification No 1644 ` QA/Q`'Offiicer <br />