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(' Sequoia 680 Chesapeake Drive Redwood City,CA 94063 (415) 364.9600 FAX(41 S)364-9233 <br /> 1900 Batts 00 Avenue,Suite L Concord,CA 94520 (510) 686.96FAX(510)686-9689 <br /> Analytical 819 Striker Avenue,Suite 8 Sacramento,CA 95834 (916) 921.9600 FAX(916)921.0100 <br /> ...:....:. ........_...,- ... ... .......•r•.. ...... ..:..........::::.,..::�::::•:::�r........,...........:...:�:::: ........;...:.:.5.....::...wN:n ,:...,;-,xr%::-�_?isrir N:�s`-. ...- ,:.:�. .... ... <br /> arr>::<.rrrr <br /> v';i:�r <br /> �vPactf9c �nvronrnentalGrotip ry�AClierit�'Project fD:�~�'31U-0D1.03/ �:�: <br /> 2025 Gateway Place, Suite 440 Matrix: Solid <br /> xs <br /> L <br /> Jose, Cnti99a �"w?i;4':.e.,,.;,:.ra-.:..A:.. o ..:-.:-. �..° a '•aec:a:f:W s::v;At�tc:- 'bs. <br /> rou <br /> QUALITY CONTROL DATA REPORT <br /> ANALYTE Total Recoverable <br /> Petroleum Hyd. <br /> Method: SM 5520 EF <br /> Analyst: A.Pina <br /> MS/MSD <br /> Batch* 940905427 <br /> Date Prepared: 9/6/94 <br /> Date Analyzed: 9/8/94 <br /> Instrument l.D.#: - <br /> Conc. Spiked: 1000 mg/kg <br /> Matrix Spike <br /> %Recovery: 110 <br /> Matrix Spike <br /> Duplicate% <br /> Recovery: 110 <br /> Relative% <br /> Difference: 0.0 <br /> :^i:{?f,�l r ?wd':.:lF.x:..:w:.�fi"'r'f:A' ^;�`fr':iA;lfjr v}:2r,',rvc n:�.•jtx:�+.',Y,i:.` <br /> ::.•l.{? <br /> ... ..........,::r-::,.. .v :._::. ::.•.:-.:: ::.:,,::^.ys:xs^:fih!^w......f-:'<•::.,r:f�.g.:;<?:.r:^a?r �"� ..0. ='aa- <br /> .•a:. ...v�..iN'::..: :,:.:7.... .rF ?r>� +'rc.`r r.'✓r.-:?. "Rm:.:-�. -::4??rr. <br /> j? fir. .a.1...:: :.✓.j..:... .f''. :..... :ti:......1..s^r'+::.; .,...�:.v:, .:,Yr -'j fj. ?r :.,:r:::-;:;:L;j'p <br /> :7.v. ...5::.r .:5:.S. v-4...n •:Y...:::i'::::r.:.,::>:::.:�.:. ..a. .:.v - e;S.�.(.u..,.r�fi'. -r.�s;:::,.r.:..:..Y x;,. ::r}}_`}}}j:+}:fF.,`a':>....,r.��:3 <br /> .:i......f:.:.,�::.r.:.i.9:.:�r .�:•.'��.C?'•rr:.�..>�,r�:,r.,. :+�--::2�f::fh?:::•..::..- �.>::,,�::::'S'.'F•'�r»'�r ui. �.-: .a-:. w,xx�cc <br /> �(>So,.4r. c;SY�o-':iivAfSs:-:•:r..s::o'::?o-::rdr`Sr-3Y'9�r,..xr.?r..: w.....:r.:.: or..fr{.. - <br /> % wtGar,c�.'RcS:s4i#aix::..,;-:;>tt•:an::lir.'�A::.::.:%`:'i:::.;>:x.+;f5:fNo:?w�;:.:.;.:.rcc:::'+woalio.a'.�:'o-r;&.`.rrSas.n::a�x.-'ws35R'Gfa.3':-`;r3"- <br /> LCS Batch#: <br /> Date Prepared: <br /> Date Analyzed: <br /> Instrument l.D.#: <br /> LCS% <br /> Recovery: <br /> % Recovery <br /> Control Limits: 70-110 <br /> Please Note: <br /> The LCS is a control sample of known,interferent free matrix that is analyzed using the same reagents, <br /> OU •lA ANALYTICAL preparation,and analytical methods employed for the samples. The matrix spike is an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure. k <br /> / the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br /> interference,the LCS recovery is to be used to validate the batch. <br /> Heen A. Manning <br /> Project Manager 9409054•PPP <2> <br />