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October 17,2013 Lab ID : STK 1339998 <br /> Live Oak Geo Environmental Customer : 3-16608 <br /> Quality Control- Inorganic <br /> anstftnem Mrlhnwl Dat,/ID "rope Knit+ <snu. Q( Dela DQO Nat. <br /> N Chem <br /> sante ;W-0 10/10/13211724011 LCS mg,L 20.0) 96.2°e 90-110 <br /> MS mg/L 400.0 106% 93-113 <br /> (STX1339976-002) MSD m9fL 400.0 103% 93-113 <br /> MSRPD mg/L 100.0 2.7% 14 <br /> Blank mg/1. ND <0.4 <br /> MS mg/l. 400.0 100% 93-113 <br /> (STK133"71-001) MSU mg/L 400.0 101% 93-113 <br /> MSRPD m 100.0 0.9% <4 <br /> 300.0 10/11/13:215074KD CCV ppm 20.00 92.9% 90-110 <br /> CCV Win 20.00 99.3% 90-110 <br /> Definition <br /> CCV CommutingCalibrationVmficalim-Atnly¢ed to verify the msuvment ealibminns is within entena. <br /> Blink Method Stank Prepared to vmfy that the pegnralion process is not contributing uomammanon to the sampks. <br /> LIES 1 ahont xv Connol Standard/Sample-Prcpaad to verify than the preparation process is not affecting aaalyne recovery. <br /> MS :Main.Spikoc-A random sample ta spiked with a known moma ofaonlyle.The toeoveries arc an indication of how that sample <br /> matna anrMs arialylc reamwcry. <br /> MSD Matrix Spike Duplicate of MS/MSD pair-A random sample duphcane is spiked with a known amount of analysed.The recoveries <br /> art an iehcw,.of how that sample metra aBeets analyte recovery. <br /> MSRPD MS/MSD Retauvc Percent Ih Retrace WD)- The MS¢Wave percent difl4ence is an indication of pie ision fix the prepanhon <br /> and analyns. <br /> ND Vin-ddoef Resultwas below the DQ0 hst,d far the anafyne. <br /> Et2mQuaddy0blixtivu-this in the criteria a ;oat which the alit c ntrul daW is cum <br /> Page 7 of 7 <br />