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GeoAnalytical Laboratories;, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209)572-0900 Fax (209) 572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Report# K074-16 Oxygenates Date: 3/30/99 <br /> Semco Project: Shell Station 1360 Escalon Ave. Escalon Date Recd: 3/15/99 <br /> 1217 S 7th Street Date Started: 3/19/99 <br /> Modesto CA 95351PO# Date Completed: 3/20/99 <br /> Date Sampled: 3/15/99 <br /> Sampler: R Chrun(Geo) <br /> Sample ID Lab ID MDL Method Analyte Results Units <br /> TK-2 West @ 15' K20996 10 8260 Methyl tertiary-Butyl Ether(MTBE) 160 µg/Kg <br /> 10 Ethanol ND <br /> 100 tertiary-Butanol ND <br /> 10 Di-isopropyl ether(DIPS) ND <br /> 10 Ethyl tertiary-Butyl Ether (ETBE) ND <br /> 10 tertiary-Amyl Methyl Ether(TAME) ND <br /> TK-2 West Side Wall @ 10' K20997 10 8260 Methyl tertiary-Butyl Ether(MTBE) 68 µg/Kg <br /> 10 Ethanol ND <br /> 100 tertiary-Butanol 2700 <br /> 10 Di-isopropyl ether(DIPE) ND <br /> 10 Ethyl tertiary-Butyl Ether (ETBE) ND <br /> 10 tertiary-Amyl Methyl Ether(TAME) ND <br /> TK-3 East @ 15' K20998 10 8260 Methyl tertiary-Butyl Ether(MTBE) ND µg/Kg <br /> 10 Ethanol ND <br /> 100 tertiary-Butanol ND <br /> 10 Di-isopropyl ether(DIPE) ND <br /> 10 Ethyl tertiary-Butyl Ether (ETBE) ND <br /> 10 tertiary-Amyl Methyl Ether(TAME) ND <br /> TK-3 West @ 16' K20999 10 8260 Methyl tertiary-Butyl Ether(MTBE) ND µg/Kg <br /> 10 Ethanol ND <br /> 100 tertiary-Butanol ND <br /> 10 Di-isopropyl ether(DIPE) ND <br /> 10 Ethyl tertiary-Butyl Ether (ETBE) ND <br /> 10 tertiary-Amyl Methyl Ether(TAME) ND <br /> Syl a Krenn Donna 1 e er <br /> Chemist Certification # 1157 Laboratory Director <br />