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GeoAnalytical Laboratories Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax (209)572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Report# K077-06 Date: 3/25/99 <br /> Semco Project: Shell Station 1360 Escalon Ave. Escalon, Date Rec'd: 3/18/99 <br /> 1217 S 7th Street CA Date Started: 3/24/99 <br /> Date Completed: 3/25/99 <br /> Modesto CA 95351 PO# <br /> Date Sampled: 3/18/99 <br /> Sampler: R Chrun(Geo) <br /> Detection <br /> Sample ID Lab ID Limit Method Analyte Results Units <br /> PL#1 at 21/2 ft K21012 10 8260 Methyl tertiary-Butyl Ether(MTBE) ND pg/Kg <br /> 10 Ethanol ND <br /> 100 tertiary-Butanol ND <br /> 10 Di-isopropyl ether(DIPE) ND <br /> 10 Ethyl tertiary-Butyl Ether(ETBE) ND <br /> 10 tertiary-Amyl Methyl Ether(TAME) ND <br /> PL#2 at 3 ft K21013 10 8260 Methyl tertiary-Butyl Ether(MTBE) ND pg/Kg <br /> 10 Ethanol ND <br /> 100 tertiary-Butanol ND <br /> 10 Di-isopropyl ether(DIPE) ND <br /> 10 Ethyl tertiary-Butyl Ether(ETBE) ND <br /> 10 tertiary-Amyl Methyl Ether(TAME) ND <br /> PL#3 at 3 ft K21014 10 8260 Methyl tertiary-Butyl Ether(MTBE) ND pg/Kg <br /> 10 Ethanol ND <br /> 100 tertiary-Butanol ND <br /> 10 Di-isopropyl ether(DIPE) ND <br /> 10 Ethyl tertiary-Butyl Ether (ETBE) ND <br /> 10 tertiary-Amyl Methyl Ether(TAME) ND <br /> PL#4 at 3 ft K21015 10 8260 Methyl tertiary-Butyl Ether(MTBE) ND pg/Kg <br /> 10 Ethanol ND <br /> 100 tertiary-Butanol ND <br /> 10 Di-isopropyl ether(DIPE) ND <br /> 10 Ethyl tertiary-Butyl Ether(ETBE) ND <br /> 10 tertiary-Amyl Methyl Ether(TAME) ND <br /> PL#5 at 3 ft K21016 10 8260 Methyl tertiary-Butyl Ether(MTBE) ND pg/Kg <br /> 10 Ethanol ND <br /> 100 tertiary-Butanol ND <br /> 10 Di-isopropyl ether(DIPE) ND <br /> 10 Ethyl tertiary-Butyl Ether (ETBE) ND <br /> 10 tertiary-Amyl Methyl Ether(TAME) ND <br /> Sylvia Krenn/,+� S Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />