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GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax (204) 572-0916 <br /> Tort# N032-04 CERTIFICATE OF ANALYSIS Date: 2/06/02 <br /> Kloberdanz &Associates Date Rec'd: 2/01/02 <br /> Date Started: 2/05/02 <br /> P.O. Box 5769$1 <br /> Project: McDowell&Davis Towing-Escalon Date Completed: 2/06/02 <br /> Modesto CA 95357 <br /> Date Sampled: 2/01/02 <br /> PO# Time: 8:53am <br /> Sample ID: MW-2 Sampler : R Azevedo(Geo) <br /> Lab ID: N301227 <br /> Method RL Analyte Results Units <br /> 8260B 0.3 Benzene 1.1 pg/L <br /> 0.3 Toluene 3.2 <br /> 0.3 Ethyl Benzene 2.1 <br /> 0.6 Total Xylenes 9.1 <br /> 1.0 Methyl tert-butyl ether (MTBE) ND <br /> 40 Ethanol ND <br /> 20 tert-Butanol ND <br /> 1.0 di-Isopropyl ether (DIPS) ND <br /> 1.0 Ethyl tert-butyl ether (ETBE) ND <br /> # 1.0 tert-Amyl methyl ether (TAME) ND <br /> 1.0 Ethylene dibromide (EDB) ND <br /> 0.5 1,2-Dichloroethane (1,2-DCA) ND <br /> s. <br /> Surrogate Amnt Spiked A=t Recovered %Recovery OC Limit% <br /> 1,2-Dichloroethane-d4 5.00 5.35 107.0 72-132 <br /> 2-Bromo-l-chloropropane 5.00 5.29 105.8 71-134 <br /> 4-Bromofluorobenzene 5.00 4.88 97.6 74-132 <br /> ario D'On iO Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />