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� r <br /> GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> �eport# M178-14 <br /> Date: 7/03/01 <br /> M.J. Kloberdanz &Associates Project: Old Shell Sation-Escalon/Quarterl Date Recd: 6/27/01 <br /> y Date Started: 7/02/01 <br /> P.O.Box 576981 Date Completed: 7/03/01 <br /> Modesto CA 95357 PO# <br /> Date Sampled: 6/27/01 <br /> Time: <br /> Sample ID: MW-1 Sampler : R Azevedo(Geo) <br /> Lab ID: M306368 <br /> Method RL Analyte Results Units <br /> 8260B 2.0 Benzene 8.5 pg/L <br /> 2.0 Toluene 46 <br /> 2.0 Ethyl Benzene 19 <br /> 4.0 Total Xylenes 43 <br /> 6.6 Methyl tert-butyl ether (MTBE) 10 <br /> 260 Ethanol ND <br /> 130 tert-Butanol ND <br /> 6.6 di-Isopropyl ether (DIPE) ND <br /> 6.6 Ethyl tert-butyl ether (ETBE) ND <br /> 6.6 tert-Amyl methyl ether (TAME) ND <br /> 6.6 Ethylene dibromide (EDB) ND <br /> 3.3 1,2-Dichloroethane (1,2-DCA) ND <br /> Surrogate Amnt Spiked Amnt Recovered %Recovery QC Limit% <br /> 1,2-Dichloroethane-d4 33 32.9 99.7 72-132 <br /> 2-Bromo-l-chloropropane 33 24.9 75.5 71-134 <br /> 4-Bromofluorobenzene 33 35.9 108.8 74-132 <br /> Mario D'Onofrio Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />