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�4lpha Analytical, Inc. 'e <br /> G 255 Glendale Ave. •Suite 21 •Sparks,Nevada 89431-5778 <br /> (775)355-1044•(775)355-0406 FAX• 1-800-283-1183 <br /> Date: Work Order: <br /> 01-Auz-03 QC Summary Report 03072125 <br /> Method Blank Type MBLK Test Code: EPA Method SW8260B <br /> File ID: C:kHPCHEM1MS011DATAk030723103072307.D Batch ID:MSIW0723A Analysis Date: 07123/2003 12:25 <br /> Sample ID: MBLK MSl W0723A Units:pg/L Run ID:GCIMSD_1_030723A Prep Date: 0712312003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> 1,2-Dibromo-3-chloropropane(DBCP) NO 3 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW82608 <br /> File ID: C:IHPCHEMIMS011DATA1030723103072304.D Batch ID:MSl W0723A Analysis Date: 07123/2003 11:09 <br /> Sample ID: LCS MSIW0723A Units; pg/L Run ID:GCIMSD_1_030723A Prep Date: 07/2312003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> 1,1-Dichloroethene 10.3 1 10 103 80 120 <br /> Benzene 10.7 0.5 10 107 83 119 <br /> Trichloroethene 10.8 1 10 108 76 127 <br /> Toluene 11.7 0.5 10 117 80 120 <br /> Chlorobenzene 11.1 1 10 111 76 124 <br /> Ethylbenzene 10.4 0.5 10 104 80 120 <br /> m,p-Xvlene 21.3 0.5 20 106 77 124 <br /> o-Xylene 10.5 0.5 10 105 77 125 <br /> Xylenes,Total 31.7 0.5 30 106 77 125 <br /> Sample Matrix Spike Type MS Test Code:EPA Method SW8260B <br /> File ID: C:IHPCHEM1MS011DATA1030723103072327.0 Batch ID:MSl W0723A Analysis Date: 07/23/2003 20:58 <br /> Sample ID: 03071901-10AMS Units: pg/L Run ID:GCIMSD_1_030723A Prep Date: 07123/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowUmit HighLimit RPD Ref Val °/RPD Qual <br /> 1,1-Dichloroethene 50.3 2.5 50 0 101 80 120 <br /> Benzene 51.8 1.3 50 0 104 83 119 <br /> Trichloroethene 48.2 2.5 50 0 96 76 127 <br /> Toluene 53 1.3 50 0 106 80 120 <br /> Chlorobenzene 50.6 2.5 50 0 101 76 124 <br /> Ethylbenzene 46.4 1.3 50 0 93 80 120 <br /> m,p-Xylene 97 1.3 100 0 97 77 124 <br /> o-Xylene 48.3 1.3 50 0 97 77 125 <br /> Xylenes,Total 145 1.3 150 0 97 77 125 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8260B <br /> File ID:C:IHPCHEMIMS011DATA1030723103072328.D Batch ID:MSl W0723A Analysis Date: 07/2312003 21:23 <br /> Sample ID: 03071901-IOAMSD Units; pg/L Run ID:GCIMSD_1_030723A Prep Date: 07/23/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowUmit HighLimit RPD Ref Val %RPD Qual <br /> 1,1-Dichloroethene 49.5 2.5 50 0 99 80 120 50.3 1.7 <br /> Benzene 50.7 1.3 50 0 101 83 119 51.76 2.15 <br /> Trichloroethene 47.9 2.5 50 0 96 76 127 48.2 0.666 <br /> Toluene 50.3 1.3 So 0 101 80 120 52.97 5.13 <br /> Chlorobenzene 48.3 2.5 So 0 97 76 124 50.6 4.75 <br /> Ethylbenzene 45.4 1.3 50 0 91 80 120 46.39 2.11 <br /> m,p-Xylene 90.9 1.3 100 0 91 77 124 96.99 6.47 <br /> o-Xylene 47.2 1.3 50 0 94 77 125 48.34 2.3 <br /> Xylenes,Total 138 1.3 150 0 92 77 125 145.3 5.07 <br /> Comments: NO-Not Detected at the Reporting Limit. D-If the spiked value is<25%of the reference value,recovery should not he calculated. <br /> S-Spike Recovery outside accepted recovery limits. M-Spike Recovery outside accepted recovery limits due to matrix. <br /> 8-Analyte detected in the associated Method Blank. <br />