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CALIFORNIA LABORATORY SERVICES <br /> 10/20/06 15:48 <br /> LFR Levine Fricke Project: Beck Prop. CLS Work Order#:CPJOd72 <br /> 4190 Douglas Blvd.;Suite 200 Project Number: 003-09246-00 <br /> Granite Bay CA,95746 Project Manager: Sal Mendoza COC#:500700,701 <br /> Organochlorine Pesticides by EPA Method 8081A- Quality Control <br /> Reposing Spike Source %REC RPD <br /> Analyte Result Umit Units Level Result %REC Limits RPD Linde Notes <br /> Batch CP08003-LUFr-DHS GCNV <br /> LCS Dup(CP08003-BSDI) Prepared: (0_/1.6_/06_ Analyzed: 10/18/06 <br /> Aldrin 15.1 1.0 pg]kg 16.7 90.4 47-132 13.4 30 <br /> gamma-BHC(Lindane) 14.9 10 16.7 89.2 56-133 15.9 30 <br /> 4,4'-DDT 17.9 15 16.7 107 46-137 1.69 30 <br /> Dieldrin 14.6 1.0 16.7 97.4 44-143 9.32 30 <br /> Endrin 14.8 IS 16.7 98.6 30-147 10.7 30 <br /> Heptachlor 15.7 10 16.7 94.0 33-148 9.33 30 <br /> Surrogate Tetrachlono-meta-xylene 8.47 6.33 102 46-139 - <br /> Swmgale:Dwachlorobipheayl 8.11 8.33 98.7 32-141 <br /> Matrix Spike(CP08003-MS I) Source:CPJ0435"59 Prepared: 10/16/06 Analyzed: 10/18/06 <br /> Aldrin 17.8 5.0 ----- _- <br /> pg/kg 16.7 ND 107 47-138 JS <br /> gemma-DHC(Lindane) 16.9 50 16.7 ND 101 38-144 35 <br /> 4,4'-DDT 24A 75 16.7 ND 146 41-157 35 <br /> Dieldrin 18.9 5.0 16.7 ND IU 46-155 35 <br /> Endrin 20.2 75 16.7 ND 121 34-t49 35 <br /> Heptachlor 20.3 50 16.7 ND 122 36-155 35 <br /> Surrogate. Tetmehloro-meta-xylene 19.0 20.8 91.3 46139 <br /> Surrogate-Deeachlorobtphenyl 15.5 20.8 113 51.141 <br /> Matrix Spike Dup(CP88003-MSD1) Source:CPJ0435-59 _ Prepared: 10/16/06 Analyzed: 10/18/06 <br /> Aldrin 16.6 5.0 pg/kg 16.7 ND 99.4 47.138 6.98 35 <br /> gemma-BHC(Lindane) 15.9 50 16.7 ND 95.2 38-144 6.10 35 <br /> 4,4'-DDT 22.1 75 16.7 ND 132 41-157 9.89 35 <br /> Dieldrin 17.6 5.0 16.7 ND 105 46-155 6.59 35 <br /> Endrin 1910 75 16.7 ND 114 34-149 6.12 35 <br /> Heptachlor 19.3 50 16.7 ND 116 36155 505 35 <br /> Surrogate:Tetrachloro-metmxylene 17.9 20.8 86.1 46139 <br /> Surrogate.-D-hlorobiphenyl 13.3 10.8 713 51-141 <br /> CA DOHS ELAP Accreditation/Registration Number 1233 <br /> 3249 Fitzgerald Road Rancho Cordova,CA 95742 www.californialab.com 916-638-7301 Fax: 916-6384510 <br />