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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> A McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccamPbell corn E-mail main@mccampbell com <br /> GEOSOLV, LLC Client Project ID Nunan/Jernigan Date Sampled 03/10/01 <br /> 643 Oregon Street Date Received 03/10/01 <br /> Sonoma,CA 95476 Client Contact Frank Goldman Date Extracted 03/13/01 <br /> Client P O Date Analyzed 03/13/01 <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 62406 62407 62408 <br /> Reporting Limit <br /> Client ID MW-I MW-2 MW-3 <br /> Matrix W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND ND ND 50 10 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND 50 10 <br /> Methyl-tett Butyl Ether(MTBE) ND ND ND 50 to <br /> tert-Amyl Methyl Ether(TAME) ND ND ND so 10 <br /> tert-Butanol ND ND ND 25 50 <br /> Methanol ND ND ND 1000 200 <br /> Ethanol ND ND ND 250 50 <br /> Surrogate Recoveries(%) <br /> Dibromoil uoromethane 114 114 116 <br /> Comments <br /> •water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment 0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />