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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-I622 <br /> http//ww-wmccatnpbelleo E-mail main@mccampbell com <br /> FGE.;S.LV, LLC Client Project ID Nunan/Jernigan Date Sampled 02/20-03/01/01 <br /> 643 Oregon Street Date Received 03/01/01 <br /> Sonoma, CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01 <br /> Client P O Date Analyzed 03/05-03/08/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 61508 <br /> Client ID MW-2 23112-24 <br /> Matrix S <br /> Reporting Limit Reporting Limit <br /> Compound Concentration* W S Compound Concentration"' W S <br /> Acetone roi ND<35 50 25 trans-l,3-Dichloropropene ND 1 0 50 <br /> Benzene ND 10 50 Ethylene dibromide ND 10 50 <br /> Bromobenzene ND 1 0 50 Ethylbenzene ND 1 0 50 <br /> Bromochloromethane ND 1 0 50 Hexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 1 0 50 lodomethane ND 10 50 <br /> Bromofonzi ND 10 50 Isopropyl benzene ND 10 50 <br /> Bromomethane ND 1 0 50 p-Isopropyl toluene ND 1 0 50 <br /> n Butyl benzene ND 10 50 Methyl butyl ketone ND 1 0 50 <br /> sec-Butyl benzene ND 1 0 50 Methylene Chloride"' ND 10 50 <br /> tert-Butyl benzene ND 10 50 Methyl ethyl ketone ND 20 10 <br /> Carbon Disulfide ND 1 0 50 Methyl isobutyl ketones ND 1 0 50 <br /> Carbon Tetrachlonde ND 1 0 50 Methyl tert-Butyl Ether(MTBE) - 1 0 50 <br /> 10 Chlorobenzene ND 1 0 50 Naphthalene ND 5 0 50 <br /> Chloroethane ND 1 0 50 n-Propyl benzene ND 1 0 5 0 <br /> 2-Chtoroethyl Vinyl Ether"' ND 1 0 50 Styrene ND 1 0 5 0 <br /> Chloroform ND 1 0k102-Tetrachloroethane ND 1 0 50 <br /> Chloromethane ND 1 02-Tetrachloroethane ND 1 0 5 0 <br /> 2 Chloratoluene ND 1 0chloroethene ND ] 0 5 0 <br /> 4-Chlorotoluene ND 1 0ne 51 ] 0 50 <br /> Dibromochtoromeihane ND 1 0 -Tnchlorobenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropropane ND 2 0 -Tnchlorobenzene ND 50 25 <br /> Dibromomethane ND 10 50 1,1,1-Trichloroethane ND 10 5 0 <br /> 12-Dichlorobenzene ND 10 5 0 1,1,2-Trichloroethane ND 10 5 0 <br /> 1,3-Dichlorobenzene ND 1 0 5 0 Tnchloroelhene ND 10 5 0 <br /> 1,4-Dichlorobenzene ND 1 0 5 0 Trichlorofluoromethane ND 1 0 5 0 <br /> Dichlorodifluoromethane ND 10 5 0 l 2,3-Tnchloropropane ND 1 0 5 0 <br /> I,1-Dichloroethane ND 1 0 5 0 1,2,4-Tnmethylbenzene ND 1 0 5 0 <br /> 1,2-Dichloroethane ND 10 5 0 1,3,5-Tnmethylbenzene ND 1 0 50 <br /> 1,1-Dichloroethene ND 10 5 0 Vinyl Acetate m ND 5 0 25 <br /> cis-1,2-Dichloroethene ND 1 0 50 Vinyl Chloride " ND to 5 0 <br /> trans-1,2-Dichloroethene ND 1 0 5 0 Xylenes,total ND 1 0 5 0 <br /> 1,2-Dichloropropane ND 10 50 Comments <br /> 1,3-Dichloropropane ND 1 0 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 50 Dibromofluoromethane 100 <br /> 1,1-Dichloropropene ND 1 0 50 Toluene-d8 106 <br /> cis-1,3-Dichloropropene ND l0 50 4-Bromofluorobenzene 108 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i) liquid sample that contains greater than ---5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br />' chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />