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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> F4 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//wwwrncc:arnpbellco E-mail main@mccampbell cote <br /> GEOSOLV,LLC Client Project 1D Nunan/7ernigan Date Sampled 02120-03/01/01 <br /> 643 Oregon Street Date Received 03/01/01 <br /> Sonoma, CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01 <br /> Client P O Date Analyzed 03/05-03108101 <br /> Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab ID 61519 <br /> Client ID MW-2 98 -99 <br /> Matnx S <br /> Reporting Lima Reporting Lima <br /> Compound Concentration* W S Compound Concentration* W S <br /> Acetone rot ND<35 50 25 trans-1,3-Dichloropropene ND 10 50 <br /> Benzene ND 1 0 50 Ethylene dibromtde ND 1 0 50 <br /> Bromobenzene ND 10 50 Ethylbenzene ND 10 50 <br /> Bromochloromethane ND 1 0 50 Hexachlorobutadiene ND 50 25 <br /> Broniodichloromethane ND to 50 lodomethane ND 10 50 <br /> Bromofonn ND 1 0 50 isopropylbenzene ND 10 50 <br /> Bromomethane ND 10 50 p-Isopropyl toluene ND 10 50 <br /> n-Butyl benzene ND 1 0 50 Methyl butyl ketone ND 10 50 <br /> sec-Butyl benzene ND 1 0 50 Methylene Chloride` ND 10 50 <br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 20 10 <br /> Carbon Disulfide ND 10 50 Methyl isobutyl ketone a ND 10 50 <br /> Carbon Tetrachloride ND 1 0 50 Methyl tert-Butyl Ether(MTBE) --- 10 50 <br /> Chlorobenzene ND 10 50 Naphthalene ND 50 50 <br /> Chloroethane ND 1 0 30 n-Propyl benzene ND 10 50 <br /> 2-Chloroethyl Vmy]Ether" IND 1 0 50 Styrene ND 1 0 50 <br /> Chloroform ND 1 0 50 1,1,1,2-Tetrachloroethane ND 1 0 50 <br /> Chloromethane ND 1 0 50 1,1,2,2-Tetrachloroethane ND 1 0 50 <br /> 2-Chlorotoluene ND 1 0 50 Tetrachloroethene ND 1 0 50 <br /> 4-Chlorotoluene ND 1 0 5 0 Toluene 79 1 0 50 <br /> Dibromochlorometbane ND 1 0 50 1,2,3-Tnchlorobenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropropane ND 20 10 1 2 4-Tnchlorobenzene ND 50 25 <br /> Dibromomethane ND 1 0 50 1,1,1-Trichloroethane ND 1 0 50 <br /> 1,2-Dichlorobenzene ND 1 0 50 1,1,2-Trichloroethane ND 1 0 50 <br /> 1,3-Dichlorobenzene ND 1 0 50 Trichloroethene ND 1 0 50 <br /> 1,4-Dichlorobenzene ND 1 0 50 Trichlorofluoromethane ND 1 0 50 <br /> Dichlorodifluoromethane ND 1 0 50 1,2,3-Tnchloropropane ND 1 0 so <br /> 1,1-Diehl oroethane ND 1 0 50 1,2,4-Tnmethylbenzene ND 1 0 50 <br /> 1,2-Dichloroethane ND 1 0 50 1,3,5-Trimethylbenzene ND 1 0 50 <br /> 1,1-Dichloroethene ND 1 0 50 Vinyl Acetate " ND 50 25 <br /> cis-1,2-Dichloroethene ND 1 0 50 Vinyl Chloride " ND 1 0 50 <br /> trans-l,2-Dichloroethene ND 1 0 50 Xylenes,total ND 10 50 <br /> 1,2-Dichloropropane ND 1 0 50 Comments <br /> 1,3-Dichloropropane ND 1 0 50 Surrogate Recoveries(%) <br /> 2,2-Dic_hl oropropane ND 1 0 50 Dibromofluoromethane 97 <br /> 1,1-51chloropropene ND 1 0 50 Toluene-d8 104 <br /> cis-1,3-Dichloropropene ND 1 0 50 4-Bronofluorobenzene 119 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in uglkg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND mcans not detected above the reporting limit NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br />' <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />