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Alpha Analytical, Inc. 255 Glendale Ave. •Suite 21 •Sparks, Nevada 89431-5778 (775) 355-1044 •(775)355-0406 FAX • 1-800-283-1183 Date: 28-Mar-03 OC Summary Report Work Order: 03031923 Method Blank Type MBLK Test Code: EPA Method SW8015 File ID: C:\HPCHEM\MSO4\DATA1030324k03032409.D Batch ID: MS4S03248 Analysis Date: 03/24/2003 11:52 Sample ID: MBLK MS4S0324A/B Units: mg/Kg Run ID:GCIMSD_4_030324A Prep Date: 03/2412003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Hight-imit RPD Ref Val %RPD. Qual TPH Purgeable ND 1 Laboratory Control Spike Type LCS Test Code: EPA Method SW8015 " File ID: C:kHPCHEMXMS04%DATAkG30324103032408.D Batch ID: MS4S0324B Analysis Date: 03/24/200311:28 Sample ID: GLCS MS4S03248 Units : mg/Kg Run ID:GC/MSD_4_030324A Prep Date: 03/2412003 Analyte Result PQL SpkVal SpkRefVal %REC LowUmit HighLimit RPD Ret Val %RPD Qual _ TPH Purgeable 8.51 1 8 106 61 144 Sample Matrix Spike Type MS Test Code: EPA Method SW8015 File ID: C:IHPCHEMIMSO4kDATA1030324103032413.0 Batch ID: MS4S0324B Analysis Date: 03/24/2003 13:26 Sample ID: 03032128-05AGS Units: mg/Kg Run ID:GC/MSD_4_030324A Prep Date: 03/24/2003 Analyte Result PQL SpkVal SpkRefVal %REC LowUnnit HighLimit RPD Ref Val %RPD Qua[ TPH Purgeable 7.35 1 8 2.171 65 61 144 .. Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8015 File ID: C:\HPCHEM\MSO41DATA\030324\03032414.D Batch ID: MS4S0324B Analysis Date: 03/24/2003 13:49 Sample ID: 03032128-05AGSD Units : mg/Kg Run ID:GCIMSD_4_030324A Prep Date: 03/24/2003 Analyte Result PQL SpkVal SpkRefVal %REC LowUmit Hight-imit RPD Ref Val °/RPD Qua[ TPH Purgeable 9.13 1 8 2.171 87 61 144 7.351 29.3 Comments: NO-Not Detected at the Reporting Limit. D-If the spiked value is<25%of the reference value,recovery should not be calculated. _ S-Spike Recovery outside accepted recovery limits. M-Spike Recovery outside accepted recovery limits due to matrix. B-Analyte detected in the associated Method Blank. _