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Alpha Analytical, Inc. <br /> ~ 255 Glendale Ave. •Suite 21 •Sparks,Nevada 89431-5778 <br /> (775)355-1044•(775)355-0406 FAX• 1-800-283-1183 <br /> Date: Work Order: <br /> 03-Jul-03 OC Summary Report 03062009 <br /> .. Method Blank Type MBLK Test Code: EPA Method SW8015 <br /> File ID: D:\MSDCHEM\MS12\DATA\030624\03062406.D Balch ID:MS12S0624B Analysis Date: 06/241200310:03 <br /> Sample ID: MBLK MS12S0624B Units:mg/Kg Run 10:GC/MSD_12_030624A Prep Date: 06124/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REG LowLimit HighLimit RPD Ref Val- %RPD Qual <br /> TPH Purqeable NO 1 <br /> Laboratory Control Spike Type LCS Test Code:EPA Method SW8015 <br /> File ID:D:(MSDCHEM%MS121DATA1030624103062408.D Batch ID:MS12S0624B Analysis Date: 06124/2003 10:44 <br /> Sample ID: GLCS MS12S0624B Units:mg/Kg Run ID:GCIMSD_12_030624A Prep Date: 06/24/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purqeable 8.62 1 8 108 61 144 <br /> w <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW8015 <br /> File ID:D:IMSDCHEM\MS121DATA1030624\03062411.D Batch.ID:MS12S0624B Analysis Date: 0612412003 11:47 <br /> Sample ID: 03062009-04AGS Units:mg/Kg Run ID:GC/MSD_12_030624A Prep Date: 0612412003 <br /> Analyte Result PQL SpkVal SpkReNal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purqeable 6.61 1 8 0 83 61 144 <br /> 4 Sample Matrix Spike Duplicate Type MSD Test Code:EPA Method SW8015 <br /> File ID: D:\MSDCHEM\MS121DATA1030624\03062412.D Batch ID:MS12S0624B Analysis Dale: 0612412003 12:08 <br /> Sample ID: 03062009-04AGSD Units:mg/Kg Run ID:GCIMSD_12_030624A Prep Date: 06124/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowt-imit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purqeable 6.56 1 8 0 82 61 144 6.609 0.683 <br /> Comments: NO-Not Detected at the Reporting Limit. D-If the spiked value is<25%of the reference value,recovery should not be calculated. <br /> S-Spike Recovery outside accepted recovery Emits. M-Spike Recovery outside accepted recovery limits due to matrix. <br /> B-Analyte detected in the associated Method Blank. <br />