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\ ('� 1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> s_ McCamgbell Analytical, Inc. Toll Fme Tcicphonc:(877)252-9262/F=(925)252-9269 <br /> ` <br /> ""en Quality Counts" hftp://www.mempbell.com mpbell.com/E-nail:rain@mccempbell.com <br /> Quality Control Report <br /> Client: Terracon WorkOrder: 170IB48 <br /> Date Prepared: 1/26/17 BatchlD: 133198 <br /> Date Analyzed: 1/26/17 Extraction Method: E300.1 <br /> Instrument: IC3 Analytical Method: E300.1 <br /> Matrix: Water Unit: mg/L <br /> Project: Macchia Winery NAI 67049 Sample 1D: MB/LCS-133198 <br /> 1701B48-001AMS/MSD <br /> QC Summary Report for E300.1 <br /> Analyte MB LCS RL SPK MB SS LCS LCS <br /> Result Result Val %REC %REC Limits <br /> Nitrate as N ND 0.976 0.10 1 - 98 85-115 <br /> Nitrate as NO3 ND 4.32 0.45 4.4 - 98 85-115 <br /> Surrogate Recovery <br /> Formate 0.109 0.109 0.10 109 109 85-115 <br /> Analyte MS MSD SPK SPKRef MS MSD MS/MSD RPD RPD <br /> Result Result Val Val %REC %REC Limits Limit <br /> Nitrate as N 2.67 2.68 1 1.680 99 100 85-115 0.353 15 <br /> Nitrate as NO3 11.8 11.9 4.4 7.441 99 100 85-115 0.353 15 <br /> Surrogate Recovery <br /> Formate 0.110 0.111 0.10 110 111 85-115 0.738 10 <br /> CDPH ELAP 1644•NELAP 4033ORELAP OV QA/QC Officer <br /> Page 5 of 10 <br />