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GeOAalytical Laboratories;11tic. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone(209) 572-0900 Fax(209) 572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Report# P014-15 Oxygenates Date: 1/17/03 <br /> Thorpe Oil Project: 530 E. Market St Date Recd: 1/14/03 <br /> PO Box 357 Date Started: 1/16/03 <br /> Lodi CA 95241 PO# Date Completed:1/16/03 <br /> Date Sampled: 1/14/03 <br /> Sampler. R.Bombaywala <br /> Sample ID Lab ID RL Method Analyte Results Units <br /> P3.#1 P200100 10 8260B Methyl tert-butyl ether(MTBE) ND jig/Kg <br /> 400 Ethanol ND <br /> 200 tert-Butanol ND <br /> 10 di-Lsopropyl ether(DIPE) ND <br /> 10 Ethyl tert-butyl ether(ETBE) ND <br /> 10 tent-Amyl methyl ether(TAME) ND <br /> I <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery QC Limit% <br /> 1,2-Dichloroethane-d4 20 24.5 1225 66-133 <br /> 2-Bromo-i-chlompropane 20 195 978 63-139 <br /> 4-Bromofluorobenzene 20 21.0 105.0 64136 <br /> P.B.#2 P200101 10 8260B Methyl tert-butyl ether(MTBE) 322 jig/Kg <br /> 400 Ethanol ND <br /> 200 tert-Butanol 4580 <br /> 10 di-Isopropyl ether(DLPE) ND <br /> 10 Ethyl tert-butyl ether(ETBE) ND <br /> 10 tert-Amyl methyl ether(TAME) 27 <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery QC Limit% <br /> 1,2-Dichloroethane-d4 20 23.1 1155 66-133 <br /> 2-Bromo-l-chloropropane 20 227 113.5 63-139 <br /> 4-Bromofluorobenzene 20 21.9 109.5 64-136 <br /> S.P.#1 Thru#5 P200102 10 8260B Methyl tert-butyl ether(MTBE) 12 jig/Kg <br /> Thru 400 Ethanol ND <br /> P200106 200 tert-Butanol ND <br /> 10 di-Isopropyl ether(DIPE) ND <br /> 10 Ethyl tert-butyl ether(ETBE) ND <br /> 10 tett-Amyl methyl ether(TAME) ND <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery QC Limit% <br /> 1,2-Dichloroethane-d4 20 21.6 108.0 66-133 <br /> 2-Bromo-l-chloropropane 20 20.4 1020 63-139 <br /> 4-Bromofluorobenzene 20 20.0 100.0 64136 <br /> Mario D'Ono o Donna*Keller <br /> Chemist Certification# 1157 Laboratory Director <br />