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CERTIFICATE OFANAL YSIS <br /> Anaiytieai Laboratory Tuesday, July 27, 1999 <br /> Advanced Geo Environmental <br /> 4005 N. Wilson Way <br /> Stockton, CA. 95205 <br /> Sample Information <br /> Sample ID: PE5528-05 Sample Type: Grab <br /> Sample Description: 3E @ 15'FT Project Name: Lodi Airport <br /> DateJTime Sampled: 7/9/99 3:33:00 PM Sample Matrix: Soil <br /> .... <br /> ANALYTICAL RESULT OA/QC REPORT <br /> .:: . , .... <br /> Date LCS Spike MS Spike a <br /> Test Parameter Method DLR Unit Result Dilution Analyzed Blank Conc. LCS% Cone MS% MSD RSD <br /> .... M. <br /> Lead(Pb) EPA 6020 1 mg/Kg 324 10 14-Jul-99 ND 002 1000% 0.025 96.0/ 104.0% 20% y <br /> TPH-Gasoline EPA 8015M/DHS 1 mg/Kg 103 1 13-Jul-99 ND 098 990% 098 11020/ 111.2% 02% s <br /> Benzene EPA 8020 5_:., ug/Kg 74 1 13-Jul-99 ND 20 955% 20 1150/ -11000, <br /> Toluene EPA 8020 5 ug/Kg 1093 1 13-Jul-99 ND 20 101.0% 20 105.0% 113.5% 1.9% <br /> .. .,, .:,�....:..:........�..,. ...:..�:,,,. .._..,,w.w..,. .:..,, ,.: 8 <br /> Ethylbenzene EPA 8020 5 ug/Kg 443 1 13-Jul-99 ND 20 9950% 20 1125% 1050°,5 1.7% <br /> c <br /> Xylenes,Total EPA 8020 5 ug/Kg 2182 1 13-Jul-99 ND 20 980% 20 1100% 1085% 03% <br /> Methyl-t-Butyl Ether(MtBE) EPA 8020 5 ug/Kg 8 1 13-Jul-99 ND 20 1050% 20 1095% 1150% 12% a <br /> nig L nnlligrmns per Liter-ppm DLR-Detection Lirmt fru the Purpose of /LSU represent relative percent d fferent thPD)betaven duplicates spike ofsamples <br /> vg/L micrograms pG <br /> Reporting. Exce tional satoP le malrices or or Duplicate ojSample <br /> = =ppb P <br /> interfereneces may result in higher detection .MS�1SD-reeasure ojlhe percent recovery efficiencies within the matrix-=Composite G=GGr rab limits <br /> LCS-measure ofthe percent recovery•ojlhe Laboratory Control Spike(LCS) <br /> RESPEC FULLYTED, <br /> Jonathan Hao V. Le,Laboratory Director <br /> EPA-Environmental Protection AgencyA•-fethod. -Pagel of t <br /> RA/-CimrdardAfallrnd fnr Rrnminatinrr nFlXofv�dltm7atwr6w.'f18WafdCf o„Ifc, A Ctnnlrtnn (:A QF9(1d TPI • (209) 462-0892 Fax: (209) 462-7935 <br />