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PRMSOH THRORG <br />Analytical Laboratory <br />3935 N. Coronado Ave, Stockton CA. 95204 Phone: (209) 477-8105 <br />Attention: Jack Bishop <br />California Tank Lines <br />3105 S. EI Dorado St <br />Stockton, CA 95206 <br />CERTIFICATE OFANALYSIS <br />Tuesday June 20, 2017 <br />Report PWe 4,4'(, <br />Metals by EPA 200 Series Methods - Quality Control <br />Precision Enviro-'rech <br />Rcpertma Spike Source 1;6R1[i: R11D <br />\nalytc Rcsmli Limit Amts Lcvcl Result "6REC Limit; RPD Limit Notes <br />Retch A['7081.5 - EPA 3020A <br />%lotricSpike (AP70815-MSI) _ <br />Source: 7060811-01 <br />Source: 7060811-01 <br />Prepared- 08-Jun-17A1><71y7.ed IiJun- 17 <br />Cadmium <br />0.0553 <br />0.00500 tltg/1. <br />0.0500 <br />ND <br />111 <br />75.125 <br />Memory <br />0.00410 <br />0.00100 <br />0.00500 <br />NO <br />82 <br />75.125 <br />Lead <br />0.051 <br />0.010 " <br />0.0500 <br />NO <br />102 <br />75.125 <br />Silver <br />0.0538 <br />0.0100 <br />0.0500 <br />NO <br />108 <br />70.125 <br />7-inc <br />0.0929 <br />0.0500 <br />0.0500 <br />0.0428 <br />100 <br />75-125 <br />Cupper <br />0,0648 <br />00500 <br />0.0500 <br />0.0151 <br />99 <br />75-125 <br />Nickel <br />0.0613 <br />n 0100 <br />0.0500 <br />0.0114 <br />100 <br />70-125 <br />Chromium <br />0.0498 <br />00100 <br />0.0500 <br />ND <br />100 <br />75-125 <br />Arsenic <br />0.0515 <br />0.0100 <br />0.0500 <br />NO <br />103 <br />80.125 <br />Matrix Spike Dup (AF70815-MSDI) <br />Source: 7060811-01 <br />Prepared:08-Jun-l7 Analyzed: 15 -Jun -17 <br />Mercury <br />0.00400 <br />0.00100 m8/t. <br />0.00500 <br />NO <br />80 <br />75-12$ <br />2 <br />20 <br />Cadmium <br />0.0556 <br />0.00500 <br />00500 <br />NO <br />III <br />75.125 <br />0,5 <br />20 <br />Land <br />0.050 <br />0.010 <br />00500 <br />ND <br />100 <br />75.125 <br />2 <br />20 <br />Silver <br />0.0550 <br />0.0100 <br />0.0500 <br />NO <br />Ito <br />70-125 <br />2 <br />20 <br />Zinc <br />0.0880 <br />0.0500 <br />0.0500 <br />0.0428 <br />91 <br />75.125 <br />5 <br />20 <br />('neper <br />0.0638 <br />0.0500 " <br />0.0500 <br />0,0151 <br />97 <br />75.125 <br />1 <br />20 <br />Nickel <br />0.0598 <br />0.0100 <br />0.0500 <br />0.0114 <br />97 <br />70-125 <br />2 <br />20 <br />Chromium <br />0.0498 <br />0.0100 <br />0.0500 <br />NO <br />100 <br />75-125 <br />0.08 <br />20 <br />Arsenic <br />0.0512 <br />0.0100 <br />0.0500 <br />ND <br />102 <br />80-125 <br />0.7 <br />20 <br />.'V1. nnllrxr*/nrs lAr l.urr ppm MR (kro..ri,rl t $-' 6�!'urluee gfftemmnx. G-Gmb Sample <br />vx I nlicrugrunr.r par Liter ppb jw Prinnal znmplY nla/rICYb Or ip/YlJYNtlCVv am}' C-c"PGrrle sample <br />Minh m higher daectlrul 4.11. <br />Cmp-Grab- Compivn of J Gmb samplr.h/nnie j1hrr Grab per u d and <br />RFSPrCTFUlA.Y SUBMITTED. cnmpmi/e wo l.sniperprioranalry•.nr <br />Jonathan H V. Le <br />Laboratory Director <br />ELAP No. 2387 email: j17vle(q-;petalab.coin Web: petallub.com Fax: (109) 516-7497 <br />