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<br /> (0fiLAB CORE LABORATORIES
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<br /> Q U A L I T Y A S S U R A N C E F 0 0 T E R
<br /> METHOD REfERENCES
<br /> (1) EPA Sot-846, Test Methods for Evaluating Solid haste, Third Edition, September 1986, and Updates 1, II, IIA, IIB, and III
<br /> (2) Standard Methods for the Examination of Yater and Wastewater, 18th Edition, 1995
<br /> (3) EPA 600/4-79-020, Methods of Chemical Analysis for Waters and Wastes, March 1983
<br /> (4) Federal Register, Friday, October 26, 1984 (40 CFR Part 136) and amendments
<br /> (5) American Society for Testing and Materials, Volumes 5 01, 5 02, 5 03, 1992
<br /> (6) EPA 600/4-89-001, Short-term Methods for Estimating the Chronic Toxicity of Effluents and Receiving Waters to Fresh
<br /> Water Organisms
<br /> (7) EPA 600/4-90-027, Methods for Measuring the Acute Toxicity of Effluent and Receiving Waters to Fresh Water and Marine
<br /> Organisms, Fourth Edition
<br /> COMMENTS
<br /> All methods of chemical analysis have a statistical uncertainty associated with the results. Unless otherwise indicated,
<br /> the data in this report are within the limits of uncertainty as specified in the referenced method Quality control
<br /> acceptance criteria are based either on limits specified in the referenced method or on actual laboratory performance
<br /> The date and time of analysis indicated on the report may not reflect the actual time of analysis for QC samples. Data
<br /> reported in the QC report may be lower than sample data due to dilution of samples into the calibration range of the analysis.
<br /> Sample concentrations for solid samples are calculated on an as received (wet) basis unless otherwise indicated Unless
<br /> otherwise indicated, volatiles by gas chromatography (GC) are reported from a single column. VolatiLes analyses by GC on low
<br /> level soils are conducted at room temperature TCLP extractions are performed at sample amounts, approved by the State of
<br /> California.
<br /> FLAGS, FOOTNOTES, AND ABBREVIATIONS (as needed)
<br /> NA = Not analyzed N.I. = Not Ignitable
<br /> /A = Not applicable S.I. = Sustains Ignition
<br /> L = Micrograms per liter I(MS) = Ignites, but does not Sustain Ignition
<br /> Mg
<br /> A = Milligrams per liter RPD = Relative Percent Difference
<br /> ND = Not detected at a value greater than the reporting limit
<br /> NC = Not calcutable due to values Lower than the detection limit
<br /> (a) = Surrogate recoveries were outside QC limits to due matrix effects
<br /> (b) = Surrogate recoveries were not calculated due to dilution of the sample below the detectable range for the surrogate
<br /> (c) = Matrix spike recoveries were outside QC limits due to matrix effects.
<br /> (d) = Relative Percent Difference (RPD) for duplicate analysis outside OC limits due to actual differences in
<br /> the sample matrix.
<br /> (e) - The limit listed for flammability indicates the upper limit for the test. Samples are not tested at temperatures
<br /> above 140 Fahrenheit since only samples which will sustain ignition at temperatures below 140 are considered
<br /> fLwty te.
<br /> (f) = Results for this hydrocarbon range did not match a typical hydrocarbon pattern. Results were quentified using a
<br /> diesel standard, however, the hydrocarbon pattern did not match a diesel pattern.
<br /> (9) = Results for this hydrocarbon range did riot match a typical hydrocarbon pattern. Results were quantified using a
<br /> gasoline standard, however, the hydrocarbon pattern did not match a gasoline pattern
<br /> (h) = High dilution due to matrix effects
<br /> QC SAMPLE IDENTIFICATIONS SUBCONTRACTED LABORATORY LOCATaI?NS
<br /> MIS - Method Blank S8 = Storage Blank Core Laboratories. Aurora, Colorado *AU
<br /> RS = Reegent Stank MS = llat-ix Spike Casper, Wyoming *CA
<br /> ICS = Initigl Calibration Blank MSD = Matrix Spike Duplicate Carson, California *CP
<br /> CC3 = Continuing Calibration Blank MD a Matrix Duplicate, Corpus Christi, Texas *CC
<br /> CS = Calibration Standard BS = Blank Spike Edison, New Jersey *ED
<br /> ICY = Initial Calibration SS a Surrogate Spike Houston, Texas (Env) *HE
<br /> verification LCS s Laboratory Control :I%Aston, Texas (Pet) *HP
<br /> CCV = Continuing Calibration Standard Indianapolis, Indiana *IN
<br /> Verification RS = Reference Standard Lake Charles, Louisiana *LC
<br /> Valparaiso, Indiana *VP
<br /> Bakersfield, California *BK-
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