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2900 - Site Mitigation Program
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Entry Properties
Last modified
11/7/2019 11:24:00 AM
Creation date
11/7/2019 11:21:25 AM
Metadata
Fields
Template:
EHD - Public
ProgramCode
2900 - Site Mitigation Program
File Section
WORK PLANS
RECORD_ID
PR0506374
PE
2960
FACILITY_ID
FA0007376
FACILITY_NAME
LUCKY STORE
STREET_NUMBER
610
Direction
W
STREET_NAME
LODI
STREET_TYPE
AVE
City
LODI
Zip
95240
CURRENT_STATUS
01
SITE_LOCATION
610 W LODI AVE
P_LOCATION
02
P_DISTRICT
004
QC Status
Approved
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' or electric rotary hammer. Once inserted to the desired depth, the probe will be rotated in a <br /> clockwise direction, or retracted slightly, opening the tip and exposing the vapor sampling ports. <br /> Soil vapor will be withdrawn from nylaflow tubing using a small calibrated syringe, connected by <br /> an on-off valve. The fust 5 dead volumes of gas will be discarded to flush the sample tubing and <br /> fill it with in-situ soil vapor. The next 20 cc of soil vapor will be withdrawn in the syringe, <br /> plugged, and transferred immediately to the onsite mobile lab for analysis. Mobile laboratory <br /> Services will be provided by Transglobal Environmental Geochemistry (TEG). High vacuums and <br /> flow rates will be avoided to minimize the chances of leakage (<200mllminute). Purging will also <br /> be minimized to ensure that samples represent VOC concentrations at the sampling tip. <br /> ' 2.3.2 Soil Gas Sample Analysis <br /> 2.3.2.1 Analytical Methods. Soil vapor samples will be analyzed for VOCs using EPA <br /> Method 8010, and analytical results will be produced on a "real time' basis. The samples will be <br /> analyzed on a gas chromatograph (GC) equipped with megabore columns and an appropriate <br /> combination of electrolytic conductivity (ELCD), photoionization (PID), flame ionization (FID) <br /> and electron capture (ECD) detectors. Detectors are be used in series to give dual detector <br /> confirmation of compounds. A surrogate compound will be added during analysis to confirm that <br /> the chromatographic retention times have not shifted. Output signals will be processed by <br /> computer chromatography software and the results entered into a laboratory computer for on-site <br /> processing and graphing. A detection limit of not more than 1 µg/L for PCE and TCE will be <br /> attained. When a measured concentration is greater than 50% of the highest concentration in the <br /> calibration range,the sample will be reanalyzed using a smaller volume or dilution. <br /> 2.3.2.2 Quality Assurance/Quality Control. The GC will be calibrated daily at the <br /> start and end of the day. A calibration standard solution, prepared from a separate source, is <br /> analyzed at the mid-point concentration immediately after the initial calibration to verify the true <br /> concentrations in the calibration standards. In order for the initial calibration to be acceptable, the <br /> response factor (RF) (the concentration divided by the chromatographic area counts) must be <br /> within+/-15% difference when compared to the average RF of the initial calibration; otherwise the <br /> instrument must be recalibrated. Acceptable continuing calibration agreement will be +/-20%. In <br /> the event that all sample analyses for the day result in non-detected concentrations of all target <br /> compounds, a laboratory control sample at the low-point calibration concentration (1 µg/L) will be <br /> analyzed at the end of the day. An ambient blank and a soil gas probe blank samples will also be <br /> analyzed at the start of each day; an ambient blank will also be analyzed when measured <br /> concentrations of a soil vapor sample is greater than 50% of the highest concentration in the <br /> 6 <br />
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