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1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> McCampbell Analytical, Inc. Toll Free Telephone:(877)252-9262/Fax:(925)252-9269 <br /> „ http://www.inecampbell.com/E-mail:main a;mccampbell.eorn <br /> "When Quality Counts <br /> Quality Control Report <br /> Client: Petralogix WorkOrder: 1807733 <br /> Date Prepared: 7/18/18 BatchID: 161771 <br /> Date Analyzed: 7/18/18 Extraction Method: E300.1 <br /> Instrument• IC3 Analytical Method: E300.1 <br /> Matrix: Water Unit: mg/L <br /> Project: Crusenberry NLS Sample ID: MB/LCS/LCSD-161771 <br /> 1807733-001 AMS/MSD <br /> QC Summary Report for E300.1 <br /> Analyte MB RL SPK MB SS MB SS <br /> Result Val %REC Limits <br /> Nitrate as N ND 0.10 <br /> Nitrate as NO3 ND 0.44 <br /> Surrogate Recovery <br /> Formate 0.114 0.10 114 85-115 <br /> Analyte LCS LCSD SPK LCS LCSD LCS/LCSD RPD RPD <br /> Result Result Val %REC %REC Limits Limit <br /> Nitrate as N 0.977 0.966 1 98 97 85-115 1.11 15 <br /> Nitrate as NO3 4.33 4.28 4.4 98 97 85-115 1.11 15 <br /> Surrogate Recovery <br /> Formate 0.113 0.113 0.10 113 113 85-115 0 10 <br /> Analyte MS MSD SPK SPKRef MS MSD MS/MSD RPD RPD <br /> Result Result Val Val %REC %REC Limits Limit <br /> Nitrate as N 2.55 2.56 1 1.439 111 113 85-115 0.493 15 <br /> Nitrate as NO3 11.3 11.4 4.4 6.373 112 113 85-115 0.493 15 <br /> Surrogate Recovery <br /> Formate 0.112 0.113 0.10 112 113 85-115 1.23 10 <br /> CA ELAP 1644•NELAP 4033ORELAP <br /> Page 4 of 8 <br />