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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Report <br /> Client: Equiva Services ServiceRequest: S9901977 <br /> Project: SAP:121258/hicident:88870583 Date Collected: 6/29/99 <br /> Sample Matrix: Soil Date Received: 6/30/99 <br /> BTEX and TPH as Gasoline <br /> Sample Name: SP-lAB COMP Units: mg/Kg(ppm) <br /> Lab Code: 59901977-037 Basis: Wet <br /> Test Notes: <br /> Prep Analvsis Dilution Date Date Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Notes <br /> Methyl tert-Butyl Ether EPA 5030 8020 0.05 1 7/1/99 7/2/99 ND <br /> Benzene EPA 5030 8020 0.005 1 7/1/99 7/2/99 ND <br /> Toluene EPA 5030 8020 0.005 1 7/1/99 7/2/99 ND <br /> Ethylbenzene EPA 5030 8020 0.005 1 7/1/99 7/2/99 ND <br /> Xvlenes,Total EPA 5030 8020 0.005 1 7/1/99 7/2/99 ND <br /> Approved By: Date: " <br /> IS22/020597p , <br /> Page 17 <br />