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COLUMBIA ANALYTICAL SERVICES; <br /> QA/QC Report <br /> Client: Equiva Services Service Request: 59901977 <br /> Project: SAP:121258/Incident:88870583 Date Collected: NA <br /> Sample Matrix: Soil Date Received: NA <br /> Date Extracted: 6/30/99 <br /> Date Analyzed: 7/6/99 <br /> Matrix Spike/Duplicate Matrix Spike Summary <br /> TPH as Diesel <br /> Sample Name: SPA A Units: mg/Kg(ppm) <br /> Lab Code: S9901977-OO1MS, 59901977-OOIDMS Basis: Wet <br /> Test Notes: <br /> Percent Recovery <br /> CAS Relative <br /> Prep Analysis Spike Level Sample Spike Result Acceptance Percent Result <br /> Analyte Method Method MRL MS DMS Result MS DMS MS DMS Limits Difference Notes <br /> TPH as Diesel LUFT California DHS LUFT 1 100 100 27 118 104 91 77 28-157 13 <br /> Approved By: Date: <br /> DMS/020597p <br /> Page 7 <br />