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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Report <br /> Client: Equiva Services Service Request: 59901977 <br /> Project: SAP:121258/lncident:88870583 Date Collected: 6/29/99 <br /> Sample Matrix: Soil Date Received: 6/30/99 <br /> TPH as Diesel <br /> Prep Method: LUFT Units: mg/Kg(ppm) <br /> Analysis Method: California DHS LUFT Basis: Wet <br /> Test Notes: <br /> Dilution Date Date Result <br /> Sample Name Lab Code MRL Factor Extracted Analyzed Result Notes <br /> SP-IA 59901977-001 1 1 6/30/99 7/6/99 27 D2 <br /> SP-IB 59901977-002 1 1 6/30/99 7/6/99 64 <br /> SP-2A S9901977-003 1 1 6/30/99 7/6/99 38 <br /> SP-2B 59901977-004 1 1 6/30/99 7/6/99 12 <br /> SP-3A 59901977-005 1 1 6/30/99 7/6/99 4 D2 <br /> SP-3B 59901977-006 1 1 6/30/99 7/6/99 6 <br /> SP-4A S9901977-007 1 1 6/30/99 7/6/99 9 <br /> SP-4B 59901977-008 1 1 6/30/99 7/6/99 ND <br /> SP-5A S9901977-009 1 1 6/30/99 7/6/99 13 <br /> SP-5B S9901977-010 1 1 6/30/99 7/7/99 5 <br /> SP-6A 59901977-011 1 I 6/30/99 7/7/99 6 D2 <br /> SP-6B S9901977-012 1 1 6/30/99 7/7/99 11 <br /> SP-7A 59901977-013 1 1 6/30/99 7/7/99 3 D2 <br /> SP-7B 59901977-014 1 1 6/30/99 7/7/99 ND <br /> SP-8A 59901977-015 1 1 6/30/99 7/7/99 7 <br /> SP-8B S9901977-016 1 1 6/30/99 7/7/99 4 <br /> SP-9A 59901977-017 1 1 6/30/99 7/7/99 8 <br /> SP-9B 59901977-018 I 1 6/30/99 7/7/99 4 <br /> Method Blank 59900630-SBI 1 1 6/30/99 7/6/99 ND <br /> Method Blank 59900630-SB2 1 1 6/30/99 7/7/99 ND <br /> D2 The sample contains a higher boiling point hydrocarbon mixture quantitated diesel. The <br /> chromatogram does not match the typical diesel fingerprint. <br /> Approved By: Date: 7-9 -S5 <br /> IA/020597p <br />