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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Report <br /> Client: Equiva Services Service Request: 59901977 <br /> Project: SAP:121258/Incident:88870583 Date Collected: 6/29/99 <br /> Sample Matrix: Sail Date Received: 6/30/99 <br /> BTEX and TPH as Gasoline <br /> Sample Name: SP-12AB COMP Units: mg/Kg(ppm) <br /> Lab Code: 59901977-048 Basis: Wet <br /> Test Notes: <br /> Prep Analysis Dilution Date Date Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Notes <br /> Methyl tert-Butyl Ether EPA 5030 8020 0.05 1 7/1/99 7/3/99 ND <br /> Benzene EPA 5030 8020 0.005 1 7/1/99 7/3/99 ND <br /> Toluene EPA 5030 8020 0.005 1 7/1/99 7/3/99 ND <br /> Ethvlbenzene EPA 5030 8020 0.005 1 7/1/99 7/3/99 ND <br /> Xvlenes,Total EPA 5030 8020 0.005 1 7/1/99 7/3/99 0.006 <br /> Approved By: Date: <br /> IS22/020597p <br /> Pace 28 <br />