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COLUMBIA ANALYTICAL SERVICE,INC. <br /> Analytical Report <br /> Client: Equiva Services Service Request: 59901977 <br /> Project: SAP:121258/lncident:88870583 Date Collected: 6/29/99 <br /> Sample Matrix: Soil Date Received: 6/30/99 <br /> BTEX and TPH as Gasoline <br /> Sample Name: SP-16AB COMP Units: mg/Kg(ppm) <br /> Lab Code: 59901977-052 Basis: Wet <br /> Test Notes: <br /> Prep Analvsis Dilution Date Date Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Motes <br /> Methyl tent-Butyl Ether EPA 5030 8020 0.05 l 7/1/99 7/1/99 ND <br /> Benzene EPA 5030 8020 0.005 1 7/1/99 7/1/99 ND <br /> Toluene EPA 5030 8020 0.005 l 7/l/99 7/l/99 0.039 <br /> Ethylbenzene EPA 5030 8020 0.005 1 7/1/99 7/l/99 0.007 <br /> Xylenes,Total EPA 5030 8020 0.005 1 7/1/99 7/l/99 0.097 <br /> Approved By: Date: <br /> 1S22/020597p <br /> Page 32 <br />