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COLUMBIA ANALYTICAL SERVICES,L,C. <br /> QA/QC Report <br /> Client: Equiva Services Service Request: 59901977 <br /> Project: SAP:121258/Incident:88870583 Date Collected: NA <br /> Sample Matrix: Soil Date Received: NA <br /> Date Extracted: 7/5/99 <br /> Date Analyzed: 7/8/99 <br /> Matrix Spike/Duplicate Matrix Spike Summary <br /> Lead <br /> Sample Name: SP-IAB COMP Units: mg/Kg(ppm) <br /> Lab Code: 59901977-0037MS, S9901977-0037DMS Basis: Wet <br /> Test Notes: <br /> Percent Recovery <br /> CAS Relative <br /> Prep Analvsis Spike Level Sample Spike Result Acceptance Percent Result <br /> Analyte Method Method MRL MS DMS Result MS DMS MS DMS Limits Difference Notes <br /> Lead EPA 3050BM 6010A 5 100 100 ND 100 100 100 100 75-125 <1 <br /> Approved By: Date: <br /> DMS/020597p <br /> Pace 41 <br />