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Sequoia680 Chesapeake Drive Redwood C'ry,CA 94063 (650) 364 9600 FAX(650)364 9233 <br /> 404 N W�get Lane Walnut Creek CA 94598 (510) 988 9600 FAX(510)988-9673 <br /> Analytical a 19 Striker Avenue,Suite a Sacramento,CA 95834 (916) 921 9600 FAX(916)921 0100 <br /> Blaine Tech Services Client Prol ID Shell Stockton/980210-A1 Sampled 02/10/98 <br /> 1680 Rogers Avenue Sample Descript MW 2 Received 02/12/98 <br /> San,Jose, CA 95112 Matrix LIQUID <br /> Analysis Method EPA 8260 Analyzed 02/20/98 <br /> Attention Fran Thie Lab Number 9802737-02 Reported 02125198 <br /> QC Batch Number MS022098MTBEH6A <br /> Instrument ID H6 <br /> Oxygenate Compounds (EPA 8260) <br /> Analyte Detection Limit Sample Results <br /> ug/L ug/L <br /> Ethanol 500 N D <br /> t-Butanol 100 N D <br /> Methyl t-Butyl Ether (MTBE) 20 N D <br /> Di-Isopropyl Ether (DIPE) 20 N D <br /> Ethyl t-Butyl Ether (ETBE) 20 N D <br /> t-Amyl Methyl Ether (TAME) 20 N D <br /> Surrogates Control Limits % % Recovery <br /> 1,2-Dichloroethane-d4 76 114 98 <br /> Analytes reported as were not present above the stated limit of detection <br /> SEC N LYTICAL - ELAP #1210 <br /> I <br /> P er <br /> Project anagen Page 6 <br />