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SEQUOIA ANALYTICAL <br /> ' 680 Chesapeake Drive • Redwood City, CA 94063 <br /> (415) 364-9600 • FAX (415) 364-9233 <br /> Blame Tech Services, Inc Client Project ID Shell, 6131 Pacific Ave , Stockton Sampled Nov 22, 1993 <br /> 985 Timothy Drive Sample Matrix Water Received Nov 23, 1993 <br /> San Jose, CA 95133 Analysis Method EPA 5030/8015/8020 Reported Dec 6, 1993 <br /> Attention Jim Keller First Sample# 3KE5401 <br /> TOTAL PURGEABLE PETROLEUM HYDROCARBONS with BTEX DISTINCTION <br /> Reporting Sample Sample Sample Sample Sample Sample <br /> Analyte Limd I D I D. I D. I D. I D. I D <br /> ,ug/L 3KE5401 3KE5402 3KE5403 3KE5404 3KE5405 3KE5406 <br /> MW-1 MW-2 MW-3 DUP EB T8 <br /> Purgeable <br /> Hydrocarbons 50 N D 370 150 000 330 N D N D <br /> Benzene 050 N D 35 19,000 5 4 N D N D <br /> Toluene 050 N D N D 28 000 N D N D N D <br /> Ethyl Benzene 050 N D N D N D N D N D N D <br /> Total Xylenes 050 N D 1 4 15,000 0 95 N D N D <br /> Chromatogram Pattern - Non-Gas Gas Non-Gas -- - <br /> Mix Mix <br /> C&-C12 C6-C12 <br /> Quality Control Data <br /> Report Limit Multiplication Factor 1 0 1 0 SCO , 0 1 0 1 0 <br /> Date Analyzed 11/30/93 11/30/93 11/30/93 12/1/93 11/29/93 11/291/93 <br /> Instrument Identification GCHP-17 GCHP-17 GCHP-17 GCHP-3 GCHP-3 GCHP-3 <br /> Surrogate Recovery, % 101 108 97 121 100 100 <br /> (OC Limits = 70-130%) <br /> Purgeabie Hydrocarbons are quantitated against a fresh gasoline standard <br /> Analytes reported as N D were not detected above the stated reporting limit <br />�SE7ANALYTICAL <br /> . 7PZ <br /> A Penner <br /> poject Manager 3KE5401 BLA <1> <br />