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4 I <br /> •4 Sequoia 680 Chesapeake Dnve Redwood City CA 94063 (415) 364 9600 FAX(415) 364 9233 <br /> 404 N Wiget Lane Walnut Creek CA 94598 (510) 988 9600 FAX(510)988 9673 <br /> Analytical 819 Striker Avenue,Suite 8 Sacramento,CA 95834 (916) 921 9600 FAX(916)921 0100 <br /> Blaine Technical Services Client Prol ID Shell Stockton 960516-A1 - Sampled 05/16/96 <br /> 985 Timothy Drive Sample Descript MW-2 Received 05/17/96 <br /> San Jose, CA 95133 Matrix LIQUID <br /> Analysis Method 8015Mod/8020 Analyzed 05/23/96 <br /> Attention Jim Keller- Lab Number 9605C69-02 Reported OSJ28196 <br />)C Batch Number GC652396BTEX02A _ <br /> istrument ID GCHP2 <br /> Total Purgeable Petroleum Hydrocarbons (TPPH) with BTEX and MTBE <br /> Analyte Detection Limit Sample Results <br /> ug/L ug/L <br /> TPPH as Gas 50 N D <br /> Methyl t-Butyl Ether 25 N D <br /> Benzene 050 N D <br /> Toluene 050 N D <br /> Ethyl Benzene 050 N D <br /> Xylenes (Total) 050 N D <br /> Chromatogram Pattern <br /> Surrogates Control Limits % % Recovery <br /> Trifluorotoluene 70 130 104 <br /> nalytes reported as N D were not present above the stated limit of detection <br />'EQU A LYTICAL - EL4P #1210 <br /> Arf enner <br /> t Manager Page 2 <br />