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�iFNDrfim, v=.RIrrCATION LABORATORY ANALYSIS <br /> rt <br /> TANK [Aye{ TPH-G T7,,4) 37,11&^ CL HC TOTAL EDB DiETALS PCB <br /> x CONT—EN-TS 5015 3015 8020 3010 LEAD ICRP/ 8270 <br /> 8260 8260 3260 3240 7420 8240 AES or 8080 <br /> 7421 AA <br /> X X I X I <br /> �� I I I I I <br /> UNL GAS X X j 1 <br /> �" DIESEL X X <br /> ,. u ICEROSEIM X X <br /> .I.. 2$ 03 UNK FUM X X X X x <br /> l 1 <br /> PROD.OIL X X <br /> CHLOR. X X <br /> a. SOLVsVTS <br /> SOLVX X I X I I ! I <br /> E � <br /> E<� U ED OIL I X 1 X I X X I 1 X I X <br /> All aaalysa methods are designated EPA methods described in EPA SW S9,Third Edition. Thasa methods net found in <br /> F- '-5W 546,are specifically noted below. Refer to tho,swP cB LUFT Feld Manual",Appendix A-?A,Table 3-5 for detection <br /> syimiu of motor vehicle fuels (�•asoline and duel). Refer to 12-3 'Regional Board Staff Recommendations for Initial <br /> Evaluation and Investigation of UST's'for the waste and motor ofl detection Ifmits <br /> Detection Limits that remain below the MCI.,MC or Allowable Limit of the contaminant in question will be accepted, <br /> however laboratory shall utilize the most conservative method. <br /> 3"t <br /> LABORATORY ALNALYSES T RMINOLOGY: <br /> '= T?H-G' Total Petroleum Hydrocarbon,Gasoline,GCFID (5030) 8015 trod or GGMS 8260 <br /> TP:I-D Total Petroleum Hydro=boa,Diesel,GClFM (3550),3015 mod or GCIMS 3260 <br /> BTX&E Benzene,Toluene,XvIene&Ethyl Benzene,GCIPID 3020 or GOMIS 3260 <br /> CL HC Chlorinated Hydrocarbon.GChiSD 3010,GCfMS 3240 <br /> TOTAL LEAD Total lead,AA 7420, AA 7421 or ICP-AES 6010 <br /> EDB Ethylene dibromide(DHS-AB 18033),GMIS 8240(DHS-Luh) - <br /> s., GC-F1D Sas Chromatography,Flame Ionization Detection <br /> ICRP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption <br /> Spectrometry 7000. Metals:Cadmium,Chromium III and VI,Lead,Zinc and Nickel. <br /> } PCS Polychlorinated Biphenyls.GOMS 3270 or SOSO <br /> Method 3050 '. Acid digestion <br /> Method 3540 Soxhlet sample preparation ' <br /> Method.3550 Sonication sample preparation,extraction method <br /> + ?3 Method 5030 Purge and trap sample preparation <br /> w <br /> QA/QC Quality Assurance/Qualiry Control <br /> b Notes: To avoid false positive detection of benzene,benzene-free solvents are to be used. Fused capillary columns are <br /> preferred to packed columns;a packed column may be used as a'6zst cut"with'dirty'samples or once the hydrocarbons <br /> -have been-characterized and proper QA/AC is followed. <br /> -- <br /> - <br /> coDrinking water sources,EPA recommends that the 500 Series for volatile organics be used an p[efCLCRC'IO the 600 SC:IeS <br /> because the detection limits are lower the QA1QC is better. <br /> E:-i?3 033 (Rev 413191) Page 8 <br /> f <br /> Nwam <br />