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INCHCAPE TESTING SERVICES <br /> SAN JOSE LABORATORIES <br /> (408) 432-8192 <br /> ' MATRIX SPIKE REPORT <br /> ITS-SJ Sample ID 97050387M5,MD SDG# NIA <br /> Client Sample ID MW-5 Analysts <br /> ' Client Prot Number 299600 Supervisor PAS <br /> Matrix LIQUID <br /> Group# 544 <br /> prep. Analyt Instr Date Date Spike Sample Matrix % MatrixENR <br /> Analyte Units Spike Sp DupRPD Q <br /> Batch Method I D Prepared Analyzed Amount Conc Conc Rec Conc ` <br /> 'Manganese M0153 6010A ICP3 05/10/97 05/12/97 ug/L 500 2170 2540 NR 2460 ; 32 H <br /> COMMENTS NR-Not reported due to high level of analyte concentration in the sample compared to spiked amount <br /> • <br /> Inorganics- Page 4 <br />