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Inchcape Testing Services Environmental Laboratories REPORT DATE 24-OCT-1996 REPORT NUMBER D96-11581 SAMPLE SUBMITTED BY ITS/San Jose ATTENTION Ms Sue Patel PROJECT 9610146 2996 0 LABORATORY QUALITY CONTROL REPORT IANALYTE Oxygen Nitrogen Ferrous Iron ferrous Iron Iron BATCH NO 101796-1T 101796-1T 8170648 817064A 14934 LCS LOT No --- 853067F 853067E 690613 PREP METHOD EPA 3810 EPA 3810 -- --- EPA 3015 PREPARED BY --------------- --------------- ST -------------- --- -- SPF ANALYSES METHOD ASTM p1945 ASTM p1945 SM 3500-Fe D SM 3500-Fe D EPA 6010A ANALYZED BY S_S S—S BAF BAF I GGD UNITS % % mg/L mg/L kg/L ' METHOD BLANK < 0 01 < 0 01 <0 05 <0 05 < 100 SPIKE LEVEL 21 0 79 0 2 00 2 00 1000 SPK REC LIMITS 80 0 - 1�O80 - 120 80 0 - 120 80 0 - 120 80 0 - 120 SPK RPD LIMITS 20 020 0 10 0 10 0 20 0 MS RESULT NA NA NS NS 1430 MS RECOVERY % NA NA NS NS 90 0 MSD RESULT NA NA NS I NS 1370 MSD RECOVERY % NA I NA NS I NS 83 7 MS/MSD RPD % NA I NA NS I NS I 7 25 IBS RESULT 20 7 I 79 3 1 98 1 94 NA BS RECOVERY % 98 6 100 99 0 97 2 NA BSD RESULT I 20 9 I 79 1 1 94 I 1 94 I NA BSD RECOVERY % 99 5 R 100 97 2 1 97 2 NA BS/8SD RPD % 0 96 I 0.25 1 83 I 0 00 I NA DUP RPD LIMITS DUPLICATE RPD % I NA ! NA NS NS I 1 31 LCS LEVEL 21 0 79 0 2 00 I 2 00 1000 LCS REC LIMITS 80 0 - 120 80 0 120 80 0 - 120 80 0 120 80 0 - 120 LCS RESULT I SEE BS SEE_BS 1 92 i 1 92 I 890 11 LCS RECOVERY % ! S>E_BS I SEE_BS 96 2 96 0 89 0 ` SPIKE SAMPLE ID - --- RB RB + 11614-4 11r SAMPLE VALUE I < 0 0100 < 0 0100 < 0 0500 I < 0 0500 ' 529 DUP SAMPLE ID -- - -- I 11614-4 I DUP SAMPLE VAL/1 I - - I 536 i DUP SAMPLE VAL/2 --- 529 NA Not applicable SEE BS LCS and LCS Duplicate reported as BS and BSD NS — Insufficient sample available for MS/MSD BS/BSD used 1 n � ► 13 � `�