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NMW <br /> APEX ENVIROTECH, INC. <br /> STANDARD OPERATING PROCEDURE <br /> Monitoring Wells <br /> SOP - 4 <br /> SOP - 1 SAMPLE IDENTIFICATION AND CHAIN- <br /> SOIL BORING SAMPLING OF-CUSTODY PROCEDURES <br /> During drilling, sail samples for chemical analysis are collected Sample identification and chain-of-custody procedures ensure <br /> in thin-walled brass tubes,of varying diameters and lengths sample ir..egrty as y'Vil as document sample possession from <br /> (e.g.,4 or 6 inches long by 2 inches outside diameter). Three the time of collection to ultimate disposal. Each sample <br /> ar four of the selected tubes,plus a spacer tube,are set in an container submitted for analysis is labeled to identify the jab <br /> 18-inch long split-barrel sampler of the appropriate inside- number,date,time of sample collection,a sample number <br /> diameter. unique to the sample,any in-field measurements made, <br /> sampling methodology,name(s)of on-site personnel,and any <br /> Where possible,the split-barrel sampler is driven its entire other pertinent field observations also recorded on the field <br /> length either hydraulically or using a t 4 -pound drop hammer. excavation or boring log. <br /> The sampler is extracted from the borehole and the brass <br /> tubes,containing the soil samples,are removed. Upon removal Chain-of-custody farms are used to record possession of the <br /> from the sampler,the selected brass tubes are either sample from time of collection to arrival at the laboratory. <br /> immediately trimmed and capped with aluminum toil or"Teflon" During shipment,the person with custody at the samples vdll <br /> sheets and plastic caps or the samples are extruded from the relinquish them to the next person by signing the chain-0f- <br /> tubes and sealed within other appropriate,cleaned sample custody form(s)and noting the data and time. The sample <br /> containers. The samples are then hermetically sealed,labeled, control officer at the laboratory will verify sample integrity, <br /> and refrigerated for delivery,under strict chain-of-custody,to correct preservation,confirm collection in the proper <br /> the analytical laboratory. These procedures minimize the container(s),and ensure adequate volume for analysis. <br /> potential for cross-contamination and volatilization of volatile <br /> organic compounds(VOC)prior to chemical analysis. If these conditions are met,the samples will be assigned <br /> unique laboratory log numbers for identification throughout <br /> One soil sample collected at each sampling interval is analyzed analysis and reporting. The log numbers will be recorded on <br /> in the field using either a portable photoionization detector the chain-a(-custody forms and in the legally-required log book <br /> (PID), flame ionization detector,organic vapor analyzer, maintained in the laboratory. The sample description,date <br /> catalytic gas detector,or an explosimeter. The purpose of this received,client's name,and any other relevant information will <br /> field analysis is to qualitatively determine the presence or also be recorded. <br /> absence of hydrocarbons,and the samples to be analyzed at <br /> the laboratory. The soil sample is sealed in either a brass tube, <br /> glass jar,or plastic bag to allow for some volatilization of VOC. SOP - 5 <br /> The PID is then used to measure the concentrations of LABORATORY ANALYTICAL QUALITY <br /> hydrocarbons within the containers's headspace. The data is ASSURANCE AND CONTROL <br /> recorded on both field notes and the boring logs at the depth <br /> corresponding to the sampling point. In addition to routine instrument calibration,replicates,spikes, <br /> blanks,spiked blanks,and certified reference materials are <br /> Other soil samples are collected to document the soil and/or routinely analyzed at method-specific frequencies to monitor <br /> stratigraphic profile beneath the project se,and estimate the, precision and bias.Additional components of the laboratory <br /> relative permeability of the subsurface materials. All drilling Quality Assurance/Quality Control program include: 1 <br /> and sampling equipment are either steam cleaned or washed in <br /> solution and doubly rinsed in deianized water prior to use at _ 1. Participation in state and federal laboratory <br /> each site and between barehales to minimize the potential for accreditation/certification programs; <br /> cross-contamination. <br /> 2 Participation in both U.S.EPA Performance <br /> In the event the soil samples cannot be submitted to the Evaluation studies(WS and WP studies)and Inter. <br /> analytical laboratory an the same day they are collected(e.g., laboratory performance evaluation programs: <br /> due to weekends or holidays),the samples are temporarily <br /> stored until the first opportunity for submittal either on Ice In a 3. Standard operating procedures describing routine <br /> cooler,such as when in the field,or in a refrigerator at Apes and periodic instrument maintenance; <br /> office. <br /> 4. 'Out-0f-Control"/Corrective Action documentation <br /> SOP procedures;and, <br /> - 3 <br /> SOIL C LASwS I Fl CATI O N 5. Multi-level review of raw data and client reports. <br /> Sail samples are classified according to the Unified Sod ' <br /> Classification System. Representative portions of the samples SOP _ g <br /> may be submitted,under strict chain-ofcustody,to an HOLLOW-STEM AUGER MONITORING <br /> analytical laboratory for further examination and verification of WELL INSTALLATION AND <br /> the In-field classification and analysis of soil mechanical and/or DEVELOPMENT <br /> petrophysical properties. The soil types are indicated on logs <br /> of ether excavations or borings together with depths Boreholes for monitoring wells are drilled using a truck- <br /> corresponding to the sampling points and other pertinent mounted,hollcw-stem auger drill rig. The borehole diameter <br /> information. will be a minimum of 4 inchas larger than the outside diameter <br /> of the casing When installing well screon. The hollow-stem <br /> auger provides minimal interruption of drilling while permitting <br />