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0 SpargerAnalytical Laboratory Division <br /> Mobile Laboratory Division <br /> Technologyinc. Scientific Division <br /> With Automotion in Mind <br /> DHS TPH LUFT as Diesel <br /> . .....--Mar-ix-S-pike (MS) & -- - - . <br /> Matrix Spike Duplicate (MSD) <br /> TPHdiesel Analysis Report <br /> Attention: Mr. Tom Landwehr Date Sampled: Sep 17, 1998 <br /> Apex Envirotech Date Received: Sep 18, 1998 <br /> 7844 Madison Ave., Ste. 106 Date Analyzed: Sep 21, 1998 <br /> Fair Oaks, CA 95628 Invoice#: 10055SEP98 <br /> Project#: ERA02.004 Project Name: Moore Petroleum <br /> Client ID: MS/MSD LAB ID: 10055-001 MS <br /> 10055-001 M S D <br /> Matrix: Soil Dilution: <br /> Conc. Sample MS MSD MS % MSD % % RPD <br /> Name Spike Added Result Result Result Units Recovery Recovery Recovery <br /> TPHdiesel 10 220 57 110 mg/kg -1630% -1100% 63% <br /> ppb=parts per billion=ug/kg=micrograms per kilogram <br /> ppm-parts per million=mg/kg=milligrams per kilogram <br /> NO=Not Detected. Compound(s)may be present at concentrations below the detection limit <br /> Note: Poor MS/MSD recoveries due to sample matrix effect. <br /> Sep 26, 1998 <br /> R.L.James,Principal Chemist Date Reported <br /> SPARGER TECHNOLOGY ANALYTICAL LABORATORY,INC.IS CERTIFIED BY THE STATE OF CALIFORNIA <br /> DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY <br /> (Certification No.1614) <br /> 8015mss <br /> 3050 Fite Circle, Suite 112 * Sacramento, California 95827 • (996) 362-8947 a FAX(996) 362-0947 <br />