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r. Spar er Analytical Laboratory Division <br /> g ry <br /> Mobile Laboratory Division <br /> Tdchnologyinc. Scientific Division <br /> With Automation in Mind <br /> Modified EPA Method 8260 GCMS <br /> OXYGENATES <br /> Attention: Mr. Tom Landwehr Date Sampled: Sep 11, 1998 <br /> Apex Envirotech Date Received: Sep 11, 1998 <br /> 7844 Madison Ave., Ste. 106 Date Analyzed: Sep 11, 1998 <br /> Fair Oaks, CA 95628 Invoice# 10021SEP98 <br /> Project#: ERA02.004 Project Name: Moore Petroleum <br /> Client 1D: Pit-3 Soil LAB ID: 10021-004A <br /> Matrix: Soil Dilution 1: 1 <br /> Reporting <br /> Compound Name Concentration Limit Units <br /> 1.) Tertiary butanol ND 10 ug/kg <br /> 2.) Methyl-tert-butyl-ether(MTBE) ND 5.0 ug/kg <br /> 3.) Di-isopropyl ether ND 5.0 ug/kg <br /> 4.) Ethyl tertiary butyl ether ND 5.0 ug/kg <br /> 5.) Tertiary amyl methyl ether ND 5.0 ug/kg <br /> Surrogate % Recovery of 1,2-dichloroethane-d4= 99% <br /> ppb=parts per D11hon=tigiRg=micrograms per Kilogram <br /> ppm=parts per million=mg/kg=milligrams per kilogram <br /> NO=Not Detected. Compound(s)may be present at concentrations below the reporting limit <br /> Sep 15, 1998 <br /> R.L.James, Principal Chemist Date Reported <br /> i <br /> SPARGER TECHNOLOGY ANALYTICAL LABORATORY,INC.IS CERTIFIED BY THE STATE OF CALIFORNIA <br /> DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY <br /> (Certification No.151 A) <br /> 8260004.x15 <br /> 3050 Fite Circle, Suite 112 e Sacramento, Colifornio 95827 • (976) 362-8947 • FAX(916) 362-0947 <br />