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r 1' APEX ENVIRCTECH, INC. STANDARD OPERATING PROCEDURE 1 k Monitoring Wells V i SOP - 4 SOP ' 1 SAMPLE IDENTIFICATION AND CHAIN- soil E3oRIN0 SAMPLING OF-CUSTODY PROCEDURES During drilling,soil samples for chemical analysis are collected Sample identification and chain-of-custodyrocedures ensure in thin-walled brass tubes,of varying diameters and lengths P j m 9 9t sample integrty as volt as document sample possession from (e.g.,4 or 6 inches long by inches outside diameter). Three the time of collection to ultimate disposal. Each sample or four of the selected tubes,plus a spacer tube,are set in an container submitted for analysis is labeled to Identify the job it-inch long split-barrel sampler of the appropriate inside- number,date,time of sample collection,a sample number diameter. unique to the sample,any in-held measurements made, i sampling methodology,name(s)of on-site personnel,and any j Where possible,the spilt-barrel sampler is driven its entire other pertinent field observations also recorded on the field ## length either hydraulically or using a 140-pound drop hammer. excavation or boring log. The sampler is extracted from the borehole and the brass tubes,containing the soil samples,are removed. Upon removal Chain-of-custody forms are used to record possession of the from the sampler,the selected brass tubes are either sample from time of collection to arrival at the laboratory, immediately trimmed and capped wlith aluminum fail or'Tefton" During shipment,the person with custody of the samples will sheets and plastic caps or the samples are extruded from the relinquish them to the ne)t person by signing the chain-of- tubes and sealed within other appropriate,cleaned sample custody form(s)and noting the date and time. The sample- ! containers. The samples are then hermetically sealed,labeled, control officer at the laboratory will verify sample integrity, and refrigerated for delivery,under strict chain-of-custody,to correct preservation,confirm collection in the proper the analytical laboratory. These procedures minimize the container(s),and ensure adequate volume for analysis, potential for cross-contamination and volatilization of volatila organic compounds(VOC)prior to chemical analysis. If these conditions are met,the samples will be assigned unique laboratory log numbers for identification throughout One soil sample collected at each sampling interval Is analyzed analysis and reporting. The log numbers will be recorded on in the field using either a portable photoionization detector the chain-of-custody farms and in the legally-required log book (PID).flame ionization detector or organic% analyzer, 9 Pmaintained in the laboratory. The sample description,date catalytic gas detector,or an explasimeter. The purpose of this received,client's name,and an ether relevant information wi[I field analysis is to qualitatively determine tho presence or y Y5 q Y P also be recorded. absence of hydrocarbons. I hyd carbons,and the samples to be analyzed at the laboratory. The soil sample is sealed in either a brass tube, glass jar,or plastic bag to allow for some volatilization of VOC. SOP _ 5 The PID is then used to measure the concentrations of LAF3oRATORY ANALYTICAL QUALITY hydrocarbons within the containers's headspace. The data Is ASSURANCE AND CONTROL recorded on both field notes and the boring logs s at the depth Pt corresponding to the sampling point, In addition to routine instrument calibration,replicates,spikes, blanks,spiked blanks,and certified reference materials are Other soil samples are collected to document the soil andfor routinelyanalyzed a,method-s collie frequencies to monitor strati ra hie profile beneath the project stet and estimate the Yz P q g P P P 1 precision and bias. Additional components of the laboratory relative permeability of the subsurface materials. Alldrilling Qualitys i A sura nceJQualit Control oniro program include: and sampling equipment are either steam cleaned or washed In y P S solution and doubly rinsed in deionized crater prior to use at 1, Participation in state and federal laboratory each site and between boreholes to minimize the potential for accredtatioNcertification programs; cross-contamination. 2. Participation in both U.S,EPA Performance In the event the soil samples cannot be submitted to the Evaluation studies(WS and WP studies)and Inter- analytical laboratory an the same day they are collected(e.g., laboratory performance evaluation programs; due to weekends or holidays),the samples are temporarily stored until the first opportunity for submittal either on Ice In a 3• Standard operating procedures describing routine cooler,such as when In the field,or in a refrigerator at Ape)?s and periodic instrument maintenance; office. 4. 'Out-of-Control"/Corrective Action documentation procedures;and, SOP . S SOIL CLAS-51FICATION 5. Multi-level review of raw data and client reports. ' I Soil samples are classified according to the Unified Soil Classification System. Representative portions of the samples SOP _ g may be submitted,under strict chain-of-custody,to an HOLLOW-STI=-M AUGER MONITORING iCt analytical laboratory for further examination and verification of VVELL- INSTALLATION AND the in-field classification and analysis of soil mechanical andfor DEVELOPMENT petrophysical properties. The soil types are indicated on logs of ether excavations or borings together with depths Boreholes for moru2oting wells are drilled using a truck- corresponding to the sampling points and other pertinent mounted,hollow-stern auger drill rig. The borehole diameter information, will be a minimum of 4 Inches larger than the outside diameter of the casing when installing well screen. The hollow-stem auger provides minimal interruption of driltng While permitting