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Spargero Analytical Laboratory Division <br /> Mobile Laboratory Division <br /> Technolyinc. ic <br /> Scientfic Division <br /> C <br /> With Automation in Mind <br /> Modified EPA Method 8260 GCMS <br /> OXYGENATES <br /> Sampled'. Oct 19, 1999 <br /> Attention: Mr, Tom Landwehr Date Sam p <br /> Apex Envirotech Date Received: Oct 20, 1999 <br /> 7844 Madison Ave. Date Analyzed: Oct 20, 1999 <br /> Fair Oaks, CA 95628 Invoice# 11614OCT99 <br /> Project#: ERA02.004 Project Name: Moore Petroleum <br /> Bulk Plant <br /> i <br /> Client lD: MW-9-25 LAB ID: 11614-007A <br /> Matrix: Soil Dilution: 1: 1 <br /> f \ ' <br /> _ Reporting i <br /> Compound Name Concentration Limit Units <br /> _ l <br /> 1.) Tertiary butanol ND 10 ug/kg •1: <br /> 2.) Methyl-tert-butyl-ether(MTBE) 4.6 2.0 uglkg <br /> 3.) Di-isopropyl ether ND 5.0 ug/kg : <br /> 4.) Ethyl tertiary butyl ether ND 5.0 ug/kg <br /> 5.) Tertiary amyl methyl ether ND 5.0 ug/kg <br /> Surrogate % Recovery of 1,2-dichloroethane-d4 = 103% i <br /> 4 <br /> ppb=parts per billion=uglkg=micrograms per kilogram <br /> ppm=parts per million=mg/kg=mil€igrams per kilogram <br /> NO=Not Detected- Compounds}may be present at concentrations below the reporting limit. <br /> Oct 20, 1999 <br /> R.L.James, Principal Chemist Date Reported <br /> SPARGER TECHNOLOGY ANALYTICAL LABORATORY,INC.IS CERTIFIED BY THE STATE OF CALIFORNEA <br /> DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY <br /> (Certification No.1614) <br /> Oxygen ate(S).xIs <br /> 3050 Fite Circle, Suite 112 • Sacramento, Califomia 95827 • (996) 362-8947 • FAX(996) 362-0947 <br />