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x <br /> I <br /> i <br /> Spargero Analytical Laboratory Division <br /> f <br /> Technoobile Laboratory Division�y Inc.lamScientific Division <br /> With Automation in Mind <br /> EPA Method 8260 GCMS <br /> Matrix Spike (MS) and Matrix Duplicate Spike (MSD) <br /> Attention: Mr. Tom Ballard Date Sampled: Oct 28, 1999 <br /> Apex Envirotech Date Received: Oti 1999 <br /> 7844 Madison Ave. Date Analyzed: Nov 1, 1999 i <br /> Fair Oaks, CA 95628 Invoice#: 11638OCT99 <br /> Project#: ERA02.004 Project Name: Moore Petroleum <br /> Client ID: MS/MSD LAB ID: 11638-001MSIMSD <br /> Matrix: Water Dilution: 1: 1 <br /> r <br /> f <br /> Units = (ii <br /> Sample Spike MS MSD QC Limits <br /> Compound Conc Added MS MSD % Rec % Rec RPD RPD % Rec <br /> 1,1-Dichloroethene ND 50 48 45 96% 90% '6% 20 61-145 <br /> Benzene ND 50 56 55 112% 110% 2% 20 76-127 <br /> Trichloroethene ND 50 54 52 108% 104% 4% 20 71-135 <br /> Toluene ND 50 56 55 112% 110% 2% 20 76-130 <br /> i Chlorobenzene ND 50 57 55 114% 110% 4% 20 75-130 <br /> ppb=parts per billion=ugll=micregrams per Iver <br /> ppm=parts per million=ug/ml=micrograms per milliliter <br /> ND=Not Detected. Compounds)may be present at concentrations below the detection limit. <br /> Nov 1, 1999 <br /> R. L.James, Principal Chemist Date Reported <br /> SPARGER TECHNOLOGY ANALYTICAL LABORATORY,INC IS CERTIRED BY THE STATE OF CALIFORNIA <br /> i� DEPARTMENT OF HEALTH Si AS A HAZARDOUS WASTE TESTING LABORATORY <br /> (Certification No.1614) <br /> Oxygenate(W).xls <br /> 3050 Fite Circle, Suite 112 9 Sacramento, California 95827 • (916) 362-8947 • FAX(916) 362-0947 <br />