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Report Number: 32862 QC Report : Matrix Spike/ Matrix Spike Duplicate Date : 05/07/2003 Project Name : Moore Petroleum Project Number: ERA02.004-QM Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup. Sample Sample Analysis Date Percent Percent Percent Recov. Diff. Parameter Sample Value Level Level Value Value Units Method Analyzed Recov. Recov. Diff. Limit Limit TPH as Diesel Blank <50 1000 1000 962 965 ug/L M EPA 8015 4129103 96.2 96.5 0.327 70-130 25 TPH as Diesel Blank <50 1000 1000 1040 1040 ug/L M EPA 8015 516103 104 104 0.805 70-130 25 Benzene 32862-15 <0.50 40.0 40.0 39.8 38.9 uglL EPA 8260B 4124103 99.6 97.4 2.23 70-130 25 Toluene 32862-15 <0.50 40.0 40.0 39.3 39.0 uglL EPA 8260E 4124103 98.2 97.6 0.690 70-130 25 Tert-Butanol 32862-15 <5.0 200 200 211 201 uglL EPA 8260B 4124103 105 101 4.61 70-130 25 Methyl-t-Butyl Ether 32862-15 <0.50 40.0 40.0 42.3 40.6 uglL EPA 8260B 4124/03 106 101 4.17 70-130 25 Benzene 32836-04 <0.50 40.0 40.0 40.0 39.7 ug/L EPA 8260E 4124103 100 99.2 0.828 70-130 25 Toluene 32836-04 <0.50 40.0 40.0 38.9 39.0 ug/L EPA 82606 4124103 97.2 97.4 0.257 70-130 25 Tert-Butanol 32836-04 15 200 200 221 227 uglL EPA 8260B 4124103 103 106' 2.77 70-130 25 Methyl-t-Butyl Ether 32836-04 61 40.0 40.0 108 110 uglL EPA 8260B 4124/03 118 123 4.03 70-130 25 Benzene 32879-04 <0.50 40.0 40.0 40.8 40.1 uglL EPA 8260B 4127103 102 100 1.58 70-130 25 Toluene 32879-04 1.6 40.0 40.0 43.4 42.6 uglL EPA 8260B 4127103 104 102 1.84 70-130 25 Tert-Butanol 32879-04 <5.0 200 200 218 224 uglL EPA 8260E 4127103 109 112 3.06 70-130 25 Methyl-t-Butyl Ether 32879-04 0.84 40.0 40.0 49.7 48.8 uglL EPA 82608 4127103 122 120 1.86 70-130 25 Benzene 32862-14 0.93 40.0 40.0 39.5 39.6 ug/L EPA 8260B 4125103 96.5 96.6 0.0777 70-130 25 Toluene 32862-14 1.4 40.0 40.0 41.5 41.7 uglL EPA 8260B 4125103 100 101 0.348 70-130 25 Tert-Butanol 32862-14 <5.0 200 200 206 212 ug/L EPA 8260B 4125103 103 106 2.84 70-130 25 Approved By: J el Kiff KIFF ANALYTICAL, LLC ; If 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800