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r � <br /> Sequoia 6i111�a,csal,rakc Ihlve Itcdwood City,CA 94063 (40) 364-96(1(1 IAX(4 t5) 3(,4.,;233 <br /> 19(x)bates Avcnuc,Sults L Concord,CA 94520 (510) 606-9600 IAX(5 10)686 9689 <br /> Analytical 019 Strikcr Avcnuc,Sults 8 Sact mento,CA 95834 (916) 921-9600 rAX(916)921.0100 <br /> }�f Z f•'k.'AYa`N!3 ,yy??' { .°........a.....i; >yr?SiY;'.•�vF ,. .:. ° ° s eY ys tY `2. xro•r c K r. y <br /> MITI Creek ssociales Client Pro(ecl ID: old <br /> P.O. Box 130 <br /> Matrix: Solid : <br /> Milrord, CA 96121 } <br /> Atlentlon: Busse.11.J.uncalWork....�� Worrk..Uror. N: 9417079 ll 02 <br /> 110polled: Jail 1r, Ur 1 <br /> .... 9rJ5�I. <br /> .j <br /> >f s t <br /> ..... :: <br /> ;9 <br /> QUALITY CONTROL DATA REPORT <br /> Ana yle: Total Flecovereble Acenaphthene Phenanthrene Pyrene <br /> Petroleum flydrocerb. <br /> QC Ela10W IN0105954101rIA GC1230g403I0VXA 0C12,1o94031orXA M1230940310EXA <br /> [Aptaly. Method: EPA 418,1 Ern83ld EPA 8310 EPA 8310 <br /> re . Method: N/A EPA 3550 EPA 3550 EPA 3550 <br /> Analyst: K.Ffynes L.Ilaar L.Ilnar L.Haar <br /> MS/MSD #: - BLK123094 BLK123094 BLK123094 <br /> Sample Cone.: N.U. N.U. N.D. <br /> Prepared Dale: 12/30/94 12/30/94 12/30/94 <br /> Analyzed Dale: - 1/5/95 1/5/95 1/5/95 <br /> Instrument LD.#: - GCW1 GCW1 GCW1 <br /> Cone. Spiked: - 1000f1g/Kg i000pg/Kg 1000119/Kg <br /> Result: • 1100 1100 1300 <br /> MS % Recovery: - 110 110 130 <br /> Dup. Result: * 9so 1000 1200 <br /> MSD%necov.: - 99 too 120 <br /> RPD: it 9,5 8.0 <br /> RPD Limit: 0.50 0.50 0.50 <br /> %!>I�f/��;•s s? 7. »g:.n•y x•;»c;f>;.�:.:yf..v.y�n*;•>,:cy.>s}si}:n::y:,•.,.: ::.}y;.p.y.v.,:.v::,.,,,,:.....••. <br /> %!!ilri/r �/�•, %��/j�!/r �rlr�i�%IN)IGSf r S� ..< wZt4;:r,"t> ZntCX+. r,wYp t C t ^2 <br /> 1.., 3� , <br /> LCS #: LCS01o595 <br /> t <br /> Prepared Dale: 1/5/95 - <br /> Analyzed Dale: 1/5/95 - <br /> Instrumenll.D.#: Flint <br /> Cone. Spiked: 230 mg/Kg <br /> LCS Result: 230 - <br /> LCS %Recov.: 100 <br /> W140 60.150 50.150 S0-150 <br /> LCS e0-120 <br /> Control Limits <br /> *MS/MSD diluted out. <br /> Please Note: <br /> The LCS is a control sample of known,Interferent-free matrix that Is analyzed using Ilse some reagents, <br /> S ANALYTICAL preparallon,and Analyllcat melhods employed for the samples. Ilia matrix spike Is an aliquot of sample <br /> ` fortified wilh known quanlilles of rpncillo compounds and subjected to the enlhe nnalylicnl procedure. It <br /> Ilia recovery of nnntylns Iroin the rnntrix spike dons not Intl wlllih spncilled conitol 1111111s duo to mnbtx <br /> 016hllorference,tho LCS recovery Is to be used 10 valWnte the balch, <br /> uz lr <br /> i' 1ec Manager ""MS- -rix Spike,MSD=MS Duplicate,tiro=nelative%Difference 9412G79.MMM <2> <br />