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BSKANALYTICAL LABORATORIES Tony Martin Certificate of Analysis Kleinfelder Inc ELAP Certificate #1180 2825 East Myrtle Street Report Issue Date: 03/14/2002 Stockton, CA 95205-4794 BSK Submission#: 2002021048 BSK Sample ID#: 184778 Project ID: DISCO Project Desc: lst.Qtr 2002 G.W. Submission Comments: Sample Type: Liquid Date Sampled: 02/21/2002 Sample Description: MW-13 Time Sampled: 1000 Sample Comments: Date Received: 02/21/2002 Organics Prep Analysis Analyte Method Result Units PQL Dilution DLA Date Date TPH as Gasoline EPA 8015(M) ND µg/L 50 1 50 02/23/2002 02/23/2002 Benzene EPA 6020 ND gg/L 0.3 1 0.3 02/23/2002 02/23/2002 Ethylbenzene EPA 8020 ND Ag/L 0.3 1 0.3 02/23/2002 02/23/2002 Toluene EPA 8020 ND Ag/L 0.3 1 0.3 02/23/2002 02/23/2002 Total Xylenes EPA 8020 ND gg/l, 0.3 1 0.3 02/23/2002 02/23/2002 1,2-Dibromoetbanc EPA 8260 ND µg/L 5.0 1 5 02/23/2002 02/23/2002 1,2-Dichloroethane EPA 6260 ND µg/L 5.0 1 5 02/23/2002 02/23/2002 tert-Butyl Alcohol EPA 6260 ND µg/L 50 1 50 02/23/2002 02/23/2002 Surrogate ---------------------------------------------------- -------------------- � --------------------------------------------------------- Fluorobenzene EPA 8020 86.5 /o Rec 1 N/A 02/23/2002 02/23/2002 Toluene-d8 EPA 8260 96.2 %Rec - 1 N/A 02/23/2002 02/23/2002 f mg/L:Milligrams/Liter(ppm) PQL:Practical Quantitation Limit H: Analyzed outside of hold time mg/Kg:Milligrams/Kilogram(ppm) DLR; Detection Limit for Reporting P:Preliminary result Ag/L:Micrograms/Liter(ppb) :PQL x Dilution S:Suspect result. See Cover Letter for comments. µg/Kg:Micrograms/Kilogram(ppb) ND:None Detected at DLR E:Analysis performed by External laboratory. %Rec:Percent Recovered(surrogates) See External Laboratory Report attachments. } Report Authentication Code; IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIilllllllllllllllllllllllllflllHl/III IIIIIIIII IIII Page 1 of 9 [` 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559-485-6935