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BSKANALYTICAL <br /> LABORATORIES <br /> Tony Martin Certificate of Analysis <br /> Kleinfelder Inc ELAP Certificate#1180 <br /> 2825 East Myrtle Street Report Issue Date: 03/14/2002 <br /> Stockton, CA 95205-4794 <br /> BSK Submission#: 2002021048 <br /> BSK Sample ID#: 184782 <br /> Project ID: DISCO Project Desc: Ist.Qtr 2002 G.W. <br /> Submission Comments: <br /> j Sample Type: Liquid Date Sampled: 02/21/2002 <br /> } Sample Description: MW-11 S Time Sampled: 1200 <br /> Sample Comments: Date Received: 02/21/2002 <br /> l Organics <br /> Prep Analysis <br /> Analyte Method Result Units PQL Dilution DLR Date Date <br /> TPH as Gasoline EPA 8015(M) 64 Ag/L 50 I 50 03/02/2002 03/02/2002 <br /> f Benzene EPA 6020 0.45 µg/L 0.3 1 0.3 03/02/2002 03/02/2002 <br /> I Ethylbenzene EPA 8020 ND µg/L 0.3 1 0.3 03/02/2002 03/02/2002 <br /> Toluene EPA 8020 ND µg/L 0.3 1 0.3 03/02/2002 03/02/2002 <br /> Total Xylenes EPA 8020 ND µg/L 0.3 1 0.3 03/02/2002 03/02/2002 <br /> 1,2-Dibromoethane EPA 8260 ND µg/L 5.0 1 5 02/23/2002 02/23/2002 <br /> 1,2-Dichloroethane EPA 8260 180 gg/L 5.0 10 50 02/25/2002 02/25/2002 <br /> ftert-Butyl Alcohol EPA 8260 ND ltg/L 50 1 50 02/23/2002 02/23/2002 <br /> Surrogate <br /> Fluorobenzene EPA 8020 87.4 %Rec. - 1 N/A 03/02/2002 03/02/2002 <br /> Toluene-d8 EPA 8260 100.6 %Rec 1 N/A 02/23/2002 02/23/2002 <br /> J LUFT Comments <br /> TAH as Gasoline T Individual peaks inconsistent with fuel fingerprint <br /> TPH as Gasoline Individual peaks inconsistent with fuel fingerprint <br /> j <br /> } mg/L:Milligrams/Liter(ppm) PQL:Practical Quantitation Limit H:Analyzed outside of hold time <br /> mg/Kg:Milligrams/Kilogram(ppm) DLR:Detection Limit for Reporting P:Preliminary result <br /> µg/L:Micrograms/Liter(ppb) :PQL x Dilution S:Suspect result. See Cover Getter for comments. <br /> gg/Kg:Micrograms/Kilogram(ppb) ND:None Detected at DLR E:Analysis performed by External laboratory. <br /> %Rec:Percent Recovered(surrogates) See External Laboratory Report attachments. <br /> Report Authentication Code: IUIIIIIIIIIIIIIN111IIIIIINIIIIII11111IIIIiIIIIIIIIIfaIIIIIIIIIIIIIIIIIIIIIIII Page 5 of 9 <br /> 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559-485-6935 <br />