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BSKANALYTICAL LABORATORIES Tony Martin Certificate of Analysis I Kleinfelder Inc ELAP Certificate#11.80 2825 East Myrtle Street Report Issue Date. 03/14/2002 I Stockton, CA 95205-4794 f . BSK Submission#: 2002021048 BSK Sample ID#: 184785 Project ID: DISCO Project Desc: ist.Qtr 2002 G.W. Submission Comments: Sample Type: Liquid Date Sampled: 02/21/2002 Sample Description: MW-9 Time Sampled: 1400 Sample Comments: Date Received: 02/21/2002 Organics { prep Analysis Analyte Method Result Units PQL Dilution DLR Date Date TPH as Gasoline EPA 8015(M) ND gg/L 50 1 50 02/23/2002 02/23/2002 { Benzene EPA 8020 ND µg/L 0.3 1 0.3 02/23/2002 02/23/2002 t Ethylbenzene EPA 8020 ND m/L 0.3 1 0.3 02/23/2002 02/23/2002 Toluene EPA 8020 ND pg/L 0.3 1 0.3 02/23/2002 02/23/2002 I Total Xylenes EPA 8020 ND µg/L 0.3 1 0.3 02/23/2002 02/23/2002 1,2-Dibromoethane EPA 8260 ND µg/L 5.0 1 5 02/23/2002 02/23/2002 1,2-Dichloroethane EPA 8260 ND µg/L 5.0 1 5 02/23/2002 02/23/2002 tort-Butyl Alcohol EPA 8260 ND gg/L 50 1 50 02123/.2002 02/23/2002 Surrogate Fluorobenzene EPA 8020 78.0 %Rec - 1 N/A 02/23/2002 02/23/2002 Toluene-d8 EPA 8260 102 %Rec - 1 N/A 02/23/2002 02/23/2002 I � 1 mg/L:Milligrams/Liter(ppm) PQL:Practical Quantitation Limit H:Analyzed outside of hold time mg/Kg:Milligrams/Kilogram(ppm) DLR:Detection Limit for Reporting P:Preliminary result jig/L:Micrograms/Liter(ppb) :PQL x Dilution S:Suspect result. See Cover Letter for comments. µg/Kg:Micrograrbs/Kilogram(ppb) ND:None Detected at DLR E:Analysis performed by External laboratory. %Rec:Percent Recovered(surrogates) See External Laboratory Report attachments. Report Authentication Code: Iliilllllllllllllilllllllllllllllllllllllllllllllllllllllllllllllllllllillllllllllll Page 8 of 9 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559-485-6935